Positional isomer differentiation of synthetic cannabinoid JWH-081 by GC-MS/MS

2015 ◽  
Vol 50 (3) ◽  
pp. 586-591 ◽  
Author(s):  
Maiko Kusano ◽  
Kei Zaitsu ◽  
Hiroshi Nakayama ◽  
Junichi Nakajima ◽  
Kazuaki Hisatsune ◽  
...  



2020 ◽  
Vol 11 (36) ◽  
pp. 9891-9897 ◽  
Author(s):  
Kavyasree Chintalapudi ◽  
Abraham K. Badu-Tawiah

An electrocatalytic nESI MS platform enables positional isomer differentiation through the localization of CC bonds in fatty acids present in complex biofluids.



2017 ◽  
Vol 22 (2) ◽  
pp. 123-132
Author(s):  
Yusuke Haruta ◽  
Atsushi Morita ◽  
Mitsuhiko Ohtsuki ◽  
Yoko Nakazono ◽  
Hideyuki Nakayama ◽  
...  


2014 ◽  
Author(s):  
Elizabeth Disney ◽  
Kenneth B. Stoller ◽  
Ryan Vandrey


2014 ◽  
Vol 1 (4) ◽  
pp. 461-464
Author(s):  
Göksel Bayar ◽  
◽  
Hüseyin Acinikli ◽  
Sedat Çakmak ◽  
Sinan Levent Kireçç ◽  
...  


Molecules ◽  
2021 ◽  
Vol 26 (4) ◽  
pp. 793
Author(s):  
Emmanouil D. Tsochatzis ◽  
Joao Alberto Lopes ◽  
Margaret V. Holland ◽  
Fabiano Reniero ◽  
Giovanni Palmieri ◽  
...  

The rapid diffusion of new psychoactive substances (NPS) presents unprecedented challenges to both customs authorities and analytical laboratories involved in their detection and characterization. In this study an analytical approach to the identification and structural elucidation of a novel synthetic cannabimimetic, quinolin-8-yl-3-[(4,4-difluoropiperidin-1-yl) sulfonyl]-4-methylbenzoate (2F-QMPSB), detected in seized herbal material, is detailed. An acid precursor 4-methyl-3-(4,4-difluoro-1-piperidinylsulfonyl) benzoic acid (2F-MPSBA), has also been identified in the same seized material. After extraction from the herbal material the synthetic cannabimimetic, also referred to as synthetic cannabinoid receptor agonists or “synthetic cannabinoids”, was characterized using gas chromatography-mass spectrometry (GC-MS), 1H, 13C, 19F and 15N nuclear magnetic resonance (NMR) and high-resolution tandem mass spectrometry (HR-MS/MS) combined with chromatographic separation. A cheminformatics platform was used to manage and interpret the analytical data from these techniques.



Heliyon ◽  
2021 ◽  
Vol 7 (4) ◽  
pp. e06730
Author(s):  
Priyanka D. Pinky ◽  
Mohammed Majrashi ◽  
Ayaka Fujihashi ◽  
Jenna Bloemer ◽  
Manoj Govindarajulu ◽  
...  


2021 ◽  
Vol 187 ◽  
pp. 108478
Author(s):  
Chris Bladen ◽  
Somayeh Mirlohi ◽  
Marina Santiago ◽  
Mitchell Longworth ◽  
Michael Kassiou ◽  
...  


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