Controlled Acid Hydrolysis of Colominic Acid under Microwave Irradiation

1999 ◽  
Vol 267 (2) ◽  
pp. 287-293 ◽  
Author(s):  
Mou-Chi Cheng ◽  
Kung-Tsung Wang ◽  
Sadako Inoue ◽  
Yasuo Inoue ◽  
Kay-Hooi Khoo ◽  
...  
2020 ◽  
Author(s):  
Nur Rokhati ◽  
Tutuk D. Kusworo ◽  
Heru Susanto ◽  
I. Nyoman Widiasa ◽  
Nita Aryanti ◽  
...  

2001 ◽  
Vol 331 (1) ◽  
pp. 9-12 ◽  
Author(s):  
Li Kunlan ◽  
Xia Lixin ◽  
Li Jun ◽  
Pang Jun ◽  
Cao Guoying ◽  
...  

2005 ◽  
Vol 340 (13) ◽  
pp. 2150-2153 ◽  
Author(s):  
Ronge Xing ◽  
Song Liu ◽  
Huahua Yu ◽  
Zhanyong Guo ◽  
Pibo Wang ◽  
...  

2019 ◽  
Vol 249 ◽  
pp. 36-44 ◽  
Author(s):  
Zheng Chen ◽  
Xiaomin Dou ◽  
Yu Zhang ◽  
Min Yang ◽  
Dongbin Wei

1962 ◽  
Vol 41 (2) ◽  
pp. 234-246 ◽  
Author(s):  
H. J. van der Molen

ABSTRACT A procedure for the quantitative determination of 5β-pregnan-3α-ol-20-one in urine is described. After acid hydrolysis of the pregnanolone-conjugates in urine, the free steroids are extracted with toluene. Pregnanolone is isolated in a pure form as its acetate; after chromatographic separation of the free steroids on alumina, the fraction containing pregnanolone is acetylated and rechromatographed on alumina. Quantitative determination of the isolated pregnanolone-acetate is carried out with the aid of the infrared spectrum recorded by a micro KBr-wafermethod. The reliability of the method under various conditions is discussed under the headings, specificity, accuracy, precision and sensitivity. It is possible to determine 30–40 μg pregnanolone in a 24-hours urine portion with a precision of 25%.


Author(s):  
M. Alekseenko ◽  
V. Litvyak ◽  
A. Sysa ◽  
E. Hrabovska ◽  
O. Galenko

2012 ◽  
Vol 11 (12) ◽  
pp. 2313-2318
Author(s):  
Theodor Malutan ◽  
Adina Elena Panzariu

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