A local measurement technique for the study of the kinetic processes of emerging of grains or blocks of grains from the inner volume to the free surface of superplastic materials during deformation is presented and used for the case of the Cd-Zn eutectic alloy deformed at room temperature. This technique could be used to evaluate the approximate time of fracture due to fissure or cavitation growth in samples under superplastic deformation. In principle, this technique will be useful for the development of physical procedures, which allows retarding the process of formation of low mismatch angle, , between neighboring grains, process which gives place to blocks of grains which dynamically behave as units under the shear stress action. For materials with nanocrystalline structures, such processes are expected to be higher than those of the case of microcrystalline materials.
Experimental Study and Response Surface Methodology for Investigation of FSP Process