Modelling of Neural Metabolism Using 13C-NMR Spectroscopy and Metabolic Flux Analysis

2010 ◽  
pp. 101-106
Author(s):  
Ana P. Teixeira ◽  
Sónia Sá Santos ◽  
Ana I. Amaral ◽  
Nuno Carinhas ◽  
Rui Oliveira ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
13C Nmr ◽  
Metabolic Flux Analysis ◽  
Metabolic Flux ◽  
13C Nmr Spectroscopy ◽  
Flux Analysis

scholarly journals Metabolic alterations induced by ischemia in primary cultures of astrocytes: merging13C NMR spectroscopy and metabolic flux analysis

2010 ◽  
Vol 113 (3) ◽  
pp. 735-748 ◽  
Author(s):  
Ana I. Amaral ◽  
Ana P. Teixeira ◽  
Sanja Martens ◽  
Vicente Bernal ◽  
Marcos F. Q. Sousa ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Metabolic Flux Analysis ◽  
Metabolic Flux ◽  
Primary Cultures ◽  
Flux Analysis ◽  
Metabolic Alterations

Metabolic flux analysis of CHO cells in perfusion culture by metabolite balancing and 2D [13C, 1H] COSY NMR spectroscopy

2010 ◽  
Vol 12 (2) ◽  
pp. 138-149 ◽  
Author(s):  
Chetan Goudar ◽  
Richard Biener ◽  
C. Boisart ◽  
Rüdiger Heidemann ◽  
James Piret ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Metabolic Flux Analysis ◽  
Cho Cells ◽  
Metabolic Flux ◽  
Perfusion Culture ◽  
Flux Analysis ◽  
Cosy Nmr

Determination of full 13C isotopomer distributions for metabolic flux analysis using heteronuclear spin echo difference NMR spectroscopy

2000 ◽  
Vol 77 (1) ◽  
pp. 25-35 ◽  
Author(s):  
Albert A de Graaf ◽  
Matthias Mahle ◽  
Michael Möllney ◽  
Wolfgang Wiechert ◽  
Peter Stahmann ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
Metabolic Flux Analysis ◽  
Metabolic Flux ◽  
Spin Echo ◽  
Flux Analysis

Combining metabolic flux analysis tools and 13C NMR to estimate intracellular fluxes of cultured astrocytes

2008 ◽  
Vol 52 (3) ◽  
pp. 478-486 ◽  
Author(s):  
Ana P. Teixeira ◽  
Sónia Sá Santos ◽  
Nuno Carinhas ◽  
Rui Oliveira ◽  
Paula M. Alves
Keyword(s):  
13C Nmr ◽  
Metabolic Flux Analysis ◽  
Metabolic Flux ◽  
Flux Analysis ◽  
Analysis Tools ◽  
Cultured Astrocytes

scholarly journals (2S,3R,6R)-2-[(R)-1-Hydroxyallyl]-4,4-dimethoxy-6-methyltetrahydro-2H-pyran-3-ol

Molbank ◽  
10.3390/m1140 ◽  
2020 ◽  
Vol 2020 (2) ◽  
pp. M1140
Author(s):  
Jack Bennett ◽  
Paul Murphy
Keyword(s):  
Mass Spectrometry ◽  
Nmr Spectroscopy ◽  
Ir Spectroscopy ◽  
13C Nmr ◽  
Conjugate Addition ◽  
13C Nmr Spectroscopy ◽  
One Pot ◽  
1H And 13C Nmr ◽  
Esi Mass Spectrometry ◽  
The One

(2S,3R,6R)-2-[(R)-1-Hydroxyallyl]-4,4-dimethoxy-6-methyltetrahydro-2H-pyran-3-ol was isolated in 18% after treating the glucose derived (5R,6S,7R)-5,6,7-tris[(triethylsilyl)oxy]nona-1,8-dien-4-one with (1S)-(+)-10-camphorsulfonic acid (CSA). The one-pot formation of the title compound involved triethylsilyl (TES) removal, alkene isomerization, intramolecular conjugate addition and ketal formation. The compound was characterized by 1H and 13C NMR spectroscopy, ESI mass spectrometry and IR spectroscopy. NMR spectroscopy was used to establish the product structure, including the conformation of its tetrahydropyran ring.

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