Determination of the relative content of kanamycin B in kanamycin sulfate preparations by the method of PMR spectroscopy

1982 ◽  
Vol 16 (2) ◽  
pp. 161-163
Author(s):  
A. I. Chernyshev ◽  
V. S. Kartashov ◽  
A. P. Arzamastsev ◽  
S. E. Esipov
Keyword(s):  
Relative Content ◽  
Pmr Spectroscopy ◽  
Kanamycin Sulfate

Prognostic value of levels of specific autoantibodies in patients of reproductive age with endometrial polyps

2021 ◽  
pp. 33-36
Author(s):  
L. V. Tkachenko ◽  
N. I. Sviridova ◽  
I. A. Gritsenko ◽  
S. N. Maksimov
Keyword(s):  
Blood Serum ◽  
Prognostic Value ◽  
Reference Range ◽  
Relative Content ◽  
Reproductive Age ◽  
Enzyme Linked Immunosorbent Assay ◽  
Women Of Reproductive Age ◽  
Endometrial Polyps ◽  
Double Stranded Dna

The problem of endometrial polyps in women of reproductive age is one of the urgent problems of modern gynecology. The detection rate of PE according to the data of domestic and foreign scientists reaches 25–35%, and therefore they occupy a leading place in the structure of intrauterine pathology.The aim. To study the levels of specific autoantibodies (to double-stranded DNA; to TrM‑03 antigens and collagen) and to assess their prognostic value for the risk of PE formation and recurrence in patients of reproductive age.Materials and methods. Examination of 86 patients aged 18 to 45 years (average age was 34.1 ± 6.3 years), admitted for hysteroscopy, hysteroresection of PE. Study of the relative content of specific autoantibodies to double-stranded DNA; to TrM‑03 antigens and collagen in blood serum was carried out by the method of enzyme-linked immunosorbent assay using specialized reagent kits (ELI-P-Complex).Results. In the course of this study, it was found that in the overwhelming majority of cases (65.1%) PEs were manifested by various types of AMC. All patients with PE were diagnosed with a significant decrease in the level of autoantibodies to double-stranded DNA, which is a marker of apoptosis processes, as well as a statistically significant decrease in the levels of autoantibodies to platelet antigens TrM‑03. The profile of deviations in the level of autoantibodies to TrM‑03 from the reference range in the area of negative values correlated with an increase in the average level of autoantibodies to collagen.Conclusions. Determination of the levels of auto-ATs to double-stranded DNA in serum can be used as a marker for predicting the recurrent course of PE. Determination of the levels of auto-ATs to platelet antigens TrM‑03 and to collagen in blood serum can be used as markers for the development of AMC by the type of BMC or a combination of BMC and BMC in patients with endometrial polyps.

Determination of the structure of methyl-substituted bicyclo[2.2.1]heptan-2-ones by PMR spectroscopy using a paramagneticshift reagent

1975 ◽  
Vol 22 (5) ◽  
pp. 655-658
Author(s):  
�. B. Krymskaya ◽  
V. I. Moskvichev ◽  
T. F. Gavrilova ◽  
N. D. Antonova ◽  
I. S. Aul'chenko ◽  
...  
Keyword(s):  
Pmr Spectroscopy

Quantitative PMR Spectroscopy of Drigs in Pharmaceutical Forms. Determination of Fenfluramine, Diethylpropion, Methyldopa and 2-Acetoxy-4-Trifluoromethylbenzoic Acid

1988 ◽  
Vol 21 (6) ◽  
pp. 455-467 ◽  
Author(s):  
A. Mazzeo Farina ◽  
M. A. Torio ◽  
A. Doldo
Keyword(s):  
Pmr Spectroscopy

Spectral method determination of kanamycin sulfate using both gold nanoparticles and quantum dots

2013 ◽  
Vol 5 (19) ◽  
pp. 5302 ◽  
Author(s):  
Ruiyong Wang ◽  
Rui Wang ◽  
Baoyu Ge ◽  
Xuelei Jia ◽  
Zhigang Li ◽  
...  
Keyword(s):  
Quantum Dots ◽  
Gold Nanoparticles ◽  
Spectral Method ◽  
Kanamycin Sulfate

Determination of the proportions of the C1, C2, and C1a components in gentamicin by PMR spectroscopy

1979 ◽  
Vol 13 (7) ◽  
pp. 774-777
Author(s):  
A. I. Chernyshev ◽  
V. D. Kartseva ◽  
S. E. Esipov ◽  
A. P. Arzamastsev
Keyword(s):  
Pmr Spectroscopy

Green Simple Spectrophotometric Methods for Determination of Kanamycin Sulfate using Eosin and Vanillin Reagents

2019 ◽  
Vol 9 (5) ◽  
pp. 634-648 ◽  
Author(s):  
Mai M. Elnaggar ◽  
Dina A. Gawad ◽  
Tarek S. Belal
Keyword(s):  
Spectrophotometric Methods ◽  
Kanamycin Sulfate

Modification of PMR Spectroscopy Technique for Determination of the Molar Substitution in Hydroxyethyl Starch

2015 ◽  
Vol 49 (8) ◽  
pp. 559-563 ◽  
Author(s):  
N. E. Kuz’mina ◽  
S. V. Moiseev ◽  
V. I. Krylov ◽  
O. V. Knyaz’kina ◽  
V. A. Yashkir ◽  
...  
Keyword(s):  
Hydroxyethyl Starch ◽  
Spectroscopy Technique ◽  
Pmr Spectroscopy ◽  
Molar Substitution

Spectrophotometric studies of kanamycin-copper complex and determination of kanamycin sulfate using an auxiliary ligand

1978 ◽  
Vol 40 (9) ◽  
pp. 1715-1718
Author(s):  
J.K. Agrawal ◽  
S.G. Harmalkar ◽  
R. Vijayavargiya
Keyword(s):  
Copper Complex ◽  
Auxiliary Ligand ◽  
Kanamycin Sulfate

scholarly journals Age features of topography and number of intestinal endocrinocytes in domestic duck

2020 ◽  
Vol 8 (4) ◽  
pp. 251-256
Author(s):  
D. S. Makhotina ◽  
M. M. Kushch ◽  
O. Ie. Zhygalova ◽  
I. A. Fesenko
Keyword(s):  
Cross Sections ◽  
Endocrine Cells ◽  
Total Population ◽  
Postnatal Period ◽  
Relative Content ◽  
Enterochromaffin Cells ◽  
First Year ◽  
Adult Bird ◽  
Age Features

The aim of the study was to determine the features of the topography and the number of the total population of endocrinocytes and enterochromaffin cells in the intestines of ducks during the first year of the postnatal period of ontogenesis. The experiments were performed on domestic ducks (Anas platyrhynchos domesticus) of black white-breasted breed (n = 5) 9 groups: 1-, 3-, 7-, 14-, 21-days-old, 1-, 2-, 6-month-old and 1-year-old. Determination of the total population of endocrine cells (argyrophilic) and enterochromaffin (argentaffin) was performed on histological specimens made from cross-sections of the middle section of the duodenum, jejunum, ileum, cecum and rectum, stained by Masson and Grimelius. The endocrine cells of 1- and 3-days-old ducks had a «superficial» location due to insufficient formation of crypts and villi. In older birds, in the duodenum, jejunum, and ileum, both argyrophilic and argentaffin APUD cells were localized mainly in crypts, and in the cecum and rectum, they were also in the epithelial layer of the villi. During the entire observation period, the highest content of both argyrophilic and argentaffin endocrinocytes in all intestines were found in 21-days-old ducks. Already at 3-days-old age, the total number of endocrine cells in various intestines corresponded to those of an adult bird. The highest number of argyrophilic and argentaffin endocrinocytes was found in the ileum and cecum, less in the rectum and jejunum, and the smallest number was in the duodenum. Enterochromaffin cells are the most common type of endocrinocytes in the ducks’ intestines, their relative content ranged from 40.1 to 97.5%. The highest relative content of argentaffin cells at 1-, 3- and 7-day-old was observed in the duodenum, at 14-day-old – in the duodenum and colon, at 21-day-old – in the rectum, at 1- and 2-month-old in jejunum, at the age of 6 month – in the duodenum, jejunum and caecum, and at the age of 1-year-old – in the ileum and cecum. In addition to argyrophilic endocrinocytes, which were located in the epithelium, other cells were found in the loose connective tissue of the villi base, the cytoplasm of which was also intensively impregnated with silver nitrate. Such cells were smaller and mostly oval in shape. Their cytoplasm was impregnated almost evenly around the nucleus and had no polarity in the location of the granules. Probably those were mast cells, which also contain bioamines, and, as well as enteroendocrinocytes, are found in the argyrophilic reaction.

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