Gas-chromatographic determination of residual hexane in hexane-extracted soybean flakes

1965 ◽  
Vol 42 (1) ◽  
pp. 62-64 ◽  
Author(s):  
L. T. Black ◽  
G. C. Mustakas

1972 ◽  
Vol 55 (6) ◽  
pp. 1226-1227
Author(s):  
Mark A Litchman ◽  
Lewis A Turano ◽  
Ronald P Upton

Abstract A method is described for the quantitative determination of hexane in modified hop extract by head-space gas-liquid chromatography. A sample of extract is weighed into a serum vial and water-methanol solution is added. The vial is sealed tightly and heated 1 hr in a 70°C bath. A sample of the head-space gas over the solution is injected onto a Porapak Q gas chromatographic column for determination. Recovery of 2–29 ppm hexane added to potassium isohumulone was 95.5–114.8%. The method may be applicable to other hop extracts.





2005 ◽  
Vol 18 (106) ◽  
pp. 450-454 ◽  
Author(s):  
Jan Kresta ◽  
Petr Kastner ◽  
Jiří Klimeš ◽  
Věra Klimešová


2002 ◽  
Vol 15 (3) ◽  
pp. 192-195 ◽  
Author(s):  
Ramesh Sane ◽  
Mary Francis ◽  
Atul Moghe ◽  
Sachin Khedkar ◽  
Ajit Anerao


2004 ◽  
Vol 17 (5) ◽  
pp. 360-364 ◽  
Author(s):  
György Kátay ◽  
Zsolt Németh ◽  
Szilárd Szani ◽  
Oszkár Köck ◽  
Levente Albert ◽  
...  


2015 ◽  
Vol 28 (2) ◽  
pp. 152-156
Author(s):  
Irena Vovk ◽  
Nadja Gerčar ◽  
Breda Simonovska ◽  
Mihael Sok


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