Radioanalytical determination of 239+240Pu and 241Am in bioassay samples by anion exchange and extraction chromatography: Preliminary considerations about the two methods

2006 ◽  
Vol 56 (1) ◽  
pp. D195-D201 ◽  
Author(s):  
S. Ridone ◽  
D. Arginelli ◽  
G. Berton ◽  
S. Bortoluzzi ◽  
G. Canuto ◽  
...  
1984 ◽  
Vol 49 (5) ◽  
pp. 1134-1139 ◽  
Author(s):  
Zdeněk Šmejkal ◽  
Jitka Tauferová ◽  
Mária Madová ◽  
Zlatica Teplá

The method describes concentration of mercury in samples of drinking water from water mains with Hg concentration above 1.0 . 10-7 g l-1 (5.0 . 10-10mol l-1) by means of extraction chromatography on a column packed with a carrier Synachrom E-5 wetted with saturated solution of bis(diethyldithiocarbamate)copper(II) complex in 1 : 1 mixture 1,2-dichlorobenzene + cyclohexane. After elution with 3.0 mol l-1 HCl the mercury concentration in the eluate is determined by atomic absorption spectrometry - cold vapour method. Average yield of the mercury separation from the model solutions was 95.8%.


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