Influence of wheel speed during planar flow melt spinning on the microstructure and soft magnetic properties of Fe68.5Si18.5B9Nb3Cu1 ribbons

2010 ◽  
Vol 46 (3) ◽  
pp. 616-622 ◽  
Author(s):  
M. Srinivas ◽  
B. Majumdar ◽  
D. Akhtar ◽  
A. P. Srivastava ◽  
D. Srivastava
2002 ◽  
Vol 102 (2) ◽  
pp. 309-316 ◽  
Author(s):  
P. Kwapuliński ◽  
Z. Stokłosa ◽  
A. Chrobak ◽  
J. Rasek ◽  
G. Haneczok

2011 ◽  
Vol 25 (14) ◽  
pp. 1241-1251 ◽  
Author(s):  
SHEIKH MANJURA HOQUE ◽  
UMASREE DHAR ◽  
M. A. HAKIM ◽  
D. K. SAHA ◽  
HARI NARAYAN DAS

Fe -based alloy of the composition, Fe 74 Cu 0.8 Nb 2.7 Si 15.5 B 7 has been studied thoroughly in order to research the evolution of nanograins and soft magnetic properties. The composition has been significantly deviated from FINEMET type composition given by Fe 73.5 Cu 1 Nb 3 Si 13.5 B 9. It is hard to optimize composition to obtain equally good soft magnetic properties as FINEMET significantly deviating from conventional type alloy. Fe -based alloy of the composition, Fe 74 Cu 0.8 Nb 2.7 Si 15.5 B 7 has been prepared by single roller melt spinning machine. X-ray diffraction studies confirmed that the ribbon is in the amorphous state. Evolution of α- Fe ( Si ) nanograins from amorphous matrix were carried out by isothermal annealing in the temperature range from 550°C to 650°C for 1, 3, 5, 10, 20, 30, 40, 50 and 60 minutes. Frequency spectrum of real and imaginary part of complex initial permeability has been measured for the samples at different annealing conditions. Short time annealing has been proved to be more efficient than long time annealing for the samples of this composition for most of the annealing temperatures.


2003 ◽  
Vol 18 (12) ◽  
pp. 2799-2806 ◽  
Author(s):  
Akihisa Inoue ◽  
Baolong Shen

Ribbon and bulk nanocrystalline body-centered-cubic (bcc) (Fe,Co) alloys exhibiting good soft magnetic properties were synthesized in Fe71.5-xCoxB13.5Si10Nb4Cu1 system by the simple production processes of melt-spinning or casting and annealing. The glass-type alloys were formed in the Co content range below 30 at.%. These glassy alloys crystallized through two exothermic reactions. The first stage was due to the precipitation of nanoscale bcc-(Fe,Co) phase with a grain size of about 10 nm, and the second stage resulted from the decomposition of the remaining amorphous phase to α–(Fe,Co), (Fe,Co)2B, (Fe,Co)23B6, (Fe,Co)3Si, and (Fe,Co)2Nb phases. The glass transition temperature increased from 820 to 827 K with increasing Co content from 5 to 20 at.%, while the supercooled liquid region decreased slightly from 37 to 30 K because of the nearly constant crystallization temperature. By choosing the 10 at.% Co-containing alloy, we produced cylindrical glassy alloy rods 1.0 and 1.5 mm in diameter by copper mold casting. The subsequent annealing for 300 s at 883 K corresponding to the temperature just above the first exothermic peak caused the formation of nanoscale bcc-(Fe,Co) structure. The bcc-(Fe,Co) alloy rods exhibited good soft magnetic properties of 1.26 T for saturation magnetization and 5.0 A/m for coercive force, which were comparable to those for the corresponding bcc-(Fe,Co) alloy ribbon. The nanocrystalline alloy in a bulk form is encouraging for future use as a new type of soft magnetic material that requires three-dimensional shapes.


2013 ◽  
Vol 203-204 ◽  
pp. 380-385 ◽  
Author(s):  
Małgorzata Karolus

Amorphous alloys based on iron, obtained by melt spinning technique, are modern and very promising soft magnetic materials. The thermal annealing at temperatures closed to the crystallization temperature can cause an increase of magnetic permeability more than 10 times i.e. the so called enhancement of soft magnetic properties effect (ESMP). It is usually explained by formation of iron nanocrystallites in amorphous surroundings or by formation of the relaxed amorphous phase. Such a microstructure leads to averaging out of magnetic anisotropy and cause the ESMP.


2010 ◽  
Vol 41 (5) ◽  
pp. 1313-1320 ◽  
Author(s):  
D. Arvindha Babu ◽  
A.P. Srivastava ◽  
B. Majumdar ◽  
D. Srivastava ◽  
D. Akhtar

2015 ◽  
Vol 2015 ◽  
pp. 1-5 ◽  
Author(s):  
Y. F. Liang ◽  
S. Wang ◽  
H. Li ◽  
Y. M. Jiang ◽  
F. Ye ◽  
...  

Melt spinning method has been widely applied for fabrication of Fe-based amorphous/nanocrystalline ribbons in industry. Compared with Fe-based amorphous/nanocrystalline alloys, Fe-6.5wt%Si high silicon steel is of low cost and has comparable excellent soft magnetic properties. Due to higher melting point and absence of supercooled liquid region, fabrication of Fe-6.5wt%Si ribbons is very hard and is only on lab scale. In this paper, we report that large scale fabrication of Fe-6.5wt%Si ribbons was successful and microstructures, ordered structures, and mechanical and soft magnetic properties of the ribbons were investigated. Due to rapid solidification rate, the ribbons were of ultrafine grains, and low degree of order and exhibited some extent of bending and tensile ductility. After heat treatment, excellent soft magnetic properties were obtained. Due to near-zero magnetostriction, the ribbons are promising to be used in electric devices with high frequencies where low noises are required.


2001 ◽  
Vol 42 (8) ◽  
pp. 1535-1539 ◽  
Author(s):  
Akinori Kojima ◽  
Satoru Ito ◽  
Akihiro Makino ◽  
Akihisa Inoue

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