scholarly journals Stress measurement using area detectors: a theoretical and experimental comparison of different methods in ferritic steel using a portable X-ray apparatus

2016 ◽  
Vol 51 (11) ◽  
pp. 5343-5355 ◽  
Author(s):  
J. Ramirez-Rico ◽  
S.-Y. Lee ◽  
J. J. Ling ◽  
I. C. Noyan
2015 ◽  
Vol 64 (7) ◽  
pp. 567-572 ◽  
Author(s):  
Yohei FUJIMOTO ◽  
Toshiyuki MIYAZAKI ◽  
Toshihiko SASAKI

1998 ◽  
Vol 3 (4) ◽  
pp. 204-207 ◽  
Author(s):  
S. Rai ◽  
T. Jayakumar ◽  
C. Babu Rao ◽  
D. K. Bhattacharya ◽  
B. Raj

Author(s):  
J.M. Titchmarsh

The advances in recent years in the microanalytical capabilities of conventional TEM's fitted with probe forming lenses allow much more detailed investigations to be made of the microstructures of complex alloys, such as ferritic steels, than have been possible previously. In particular, the identification of individual precipitate particles with dimensions of a few tens of nanometers in alloys containing high densities of several chemically and crystallographically different precipitate types is feasible. The aim of the investigation described in this paper was to establish a method which allowed individual particle identification to be made in a few seconds so that large numbers of particles could be examined in a few hours.A Philips EM400 microscope, fitted with the scanning transmission (STEM) objective lens pole-pieces and an EDAX energy dispersive X-ray analyser, was used at 120 kV with a thermal W hairpin filament. The precipitates examined were extracted using a standard C replica technique from specimens of a 2¼Cr-lMo ferritic steel in a quenched and tempered condition.


Author(s):  
Fabian Jaeger ◽  
Alessandro Franceschi ◽  
Holger Hoche ◽  
Peter Groche ◽  
Matthias Oechsner

AbstractCold extruded components are characterized by residual stresses, which originate from the experienced manufacturing process. For industrial applications, reproducibility and homogeneity of the final components are key aspects for an optimized quality control. Although striving to obtain identical deformation and surface conditions, fluctuation in the manufacturing parameters and contact shear conditions during the forming process may lead to variations of the spatial residual stress distribution in the final product. This could lead to a dependency of the residual stress measurement results on the relative axial and circumferential position on the sample. An attempt to examine this problem is made by the employment of design of experiments (DoE) methods. A statistical analysis of the residual stress results generated through X-Ray diffraction is performed. Additionally, the ability of cold extrusion processes to generate uniform stress states is analyzed on specimens of austenitic stainless steel 1.4404 and possible correlations with the pre-deformed condition are statistically examined. Moreover, the influence of the coating, consisting of oxalate and a MoS2 based lubricant, on the X-Ray diffraction measurements of the surface is investigated.


1944 ◽  
Vol 10 (38-1) ◽  
pp. 17-22
Author(s):  
Toshio NISHIHARA ◽  
Kohei KOZIMA ◽  
Shuzi TAIRA ◽  
Yutaro KOSAKA ◽  
Takeo TOMIYASU

2007 ◽  
Vol 22 (2) ◽  
pp. 103-107 ◽  
Author(s):  
Balder Ortner

The equation ε(φ, ψ, hkl)=Fij(φ, ψ, hkl)σij can be directly deduced from Hooke’s law. It is shown that the matrix Fij(φ, ψ, hkl) which is usually called X-ray elastic factors, behaves as a second rank tensor. Since this behaviour is the only criterion for the question of whether or not it is a tensor, the F-matrix must be regarded as a second rank tensor. This allows us to make some statements about the structure of the F-matrix on the basis of Neumann’s principle, to find relationships among F-matrices in different measurement directions, and to apply the methods and strategies for the measurement of a second rank tensor. All this is shown in a few examples. It is further shown that a consistent use of the F-matrix can replace all methods for data evaluation which makes use of linear regressions and, in addition, avoids all difficulties and disadvantages of these methods. One of these disadvantages is that the sin2 ψ-method, as well as its derivatives, is generally not correct least square fits of the measured data. This is also shown in an example. The more complicated cases with stress or constitution gradients in the range of the probed volume or stress measurement after plastic deformation are not discussed.


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