Preparation and characterization of poly(ether ether ketone)/poly(ether imide) [PEEK/PEI] blends for fused filament fabrication

2021 ◽  
Author(s):  
Anouar El Magri ◽  
Khalil El Mabrouk ◽  
Sébastien Vaudreuil
Keyword(s):  
Fused Filament Fabrication ◽  
Ether Ether Ketone ◽  
Poly Ether Ether Ketone ◽  
Ether Ketone

scholarly journals Synthesis and Characterization of alumina nanofiber reinforced Poly ether ether ketone (PEEK)

2014 ◽  
Vol 7 (2) ◽  
Author(s):  
Tg Mahizatulazwa Tg Kamaruddin ◽  
Liew Kong Yong ◽  
Mohd Ridzuan Noordin
Keyword(s):  
Degree Of Crystallinity ◽  
Nano Composites ◽  
Scanning Electron Micrographs ◽  
X Ray ◽  
Alumina Nanofibers ◽  
Transmission Electron ◽  
Ether Ether Ketone ◽  
Poly Ether Ether Ketone ◽  
Ether Ketone

The effects of reinforcing Poly ether etherketone (PEEK) with alumina nanofiber have been studied. The nano-composites were prepared by first dispersing the fibre in solvent and then undertaking the synthesis of PEEK. Nanocomposite materials with 1wt.%, 2.5wt.% and 5wt.% of alumina nanofiber have been prepared successfully by dispersing the alumina nanofiber in Sulfolane as solvent and upon sonication for 30 minutes. Transmission electron microscopy and scanning electron micrographs indicated excellent dispersion and interactions between PEEK matrixes with the added alumina nanofibers. Differential scanning calorimeter shows changes in melting and crystallization point and degree of crystallinity for 1wt.% nanocomposites. The result also indicated that alumina nanofiber serves as nucleating agents in PEEK nanocomposites. The X-ray diffractogram data indicated that the crystallinity of the PEEK nanocomposites was highest for 1wt.% alumina nanofiber. The thermogravimetry analysis, shows that thermal stability for alumina nanofiber/PEEK nano-composites was enhanced compared to that of the pure PEEK.

Characterization of molecular interaionic and intraionic crosslinkable sulfonated poly(ether ether ketone-alt-benzimidazole) membrane

2011 ◽  
Vol 124 (4) ◽  
pp. 3175-3183 ◽  
Author(s):  
Jianli Wang ◽  
Hongfei Yu ◽  
Myong-Hoon Lee ◽  
Shenggang Zhang ◽  
Dehai Wang
Keyword(s):  
Ether Ether Ketone ◽  
Poly Ether Ether Ketone ◽  
Ether Ketone ◽  
Sulfonated Poly

Development and characterization of novel poly(ether ether ketone)/ZnO bionanocomposites

2014 ◽  
Vol 2 (20) ◽  
pp. 3065 ◽  
Author(s):  
Ana M. Díez-Pascual ◽  
Chunping Xu ◽  
Rafael Luque
Keyword(s):  
Ether Ether Ketone ◽  
Poly Ether Ether Ketone ◽  
Ether Ketone

Synthesis and Characterization of Novel Fluorene-Based Poly(Imino Ketone)s

2011 ◽  
Vol 335-336 ◽  
pp. 1086-1089
Author(s):  
Lin Zhang ◽  
Guan Jun Chang ◽  
Lu Bin Miao ◽  
Run Xiong Lin
Keyword(s):  
Optical Properties ◽  
Room Temperature ◽  
Main Chain ◽  
High Glass Transition Temperature ◽  
Good Solubility ◽  
Ether Ether Ketone ◽  
Poly Ether Ether Ketone ◽  
Ft Ir ◽  
Ether Ketone

Fluorene-based poly(imino ketone)s (PIKF) were designed and synthesized by reacting 1,4-Bis-(4-bromobenzoyl)-benzene and 9,9-bis(3-R-4-aminophenyl)fluorine (R: H, CH3 or F). The structures of the resulting polymers were characterized by FT-IR, 1H NMR spectroscopy and elemental analysis. The thermo and optical properties of PIKF were evaluated. Good solubility of PIKF in ordinary organic solvents such as THF and chloroform was confirmed. PIKF were amorphous at room temperature. No phase transition except for Tg was confirmed in the DSC analysis. PIKF displayed a high glass transition temperature (Tg > 215 °C) in comparison with commercially available poly(ether ether ketone) (PEEK Tg = 169 °C). The UV-vis absorption spectrum of polymers exhibited two absorption peaks around 271 nm and 369 nm; The fluorescence spectrum of the PIKF-1, 2 and PIKF-3 showed a maximum emission wavelength at 502 nm and 491 nm, respectively. These optical properties were probably related to the cardo structure of the fluorene moiety placed on the main chain.

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