Continuous Flow–Assisted Polyol Synthesis of Citric Acid Functionalized Iron Oxide Nanoparticles

2022 ◽  
Author(s):  
Nevzat Akkurt ◽  
Cem Levent Altan ◽  
Mehmet Fahri Sarac
Keyword(s):  
Iron Oxide ◽  
Citric Acid ◽  
Iron Oxide Nanoparticles ◽  
Continuous Flow ◽  
Polyol Synthesis ◽  
Oxide Nanoparticles

scholarly journals Nanocatalysis in continuous flow: supported iron oxide nanoparticles for the heterogeneous aerobic oxidation of benzyl alcohol

2013 ◽  
Vol 15 (6) ◽  
pp. 1530 ◽  
Author(s):  
David Obermayer ◽  
Alina M. Balu ◽  
Antonio A. Romero ◽  
Walter Goessler ◽  
Rafael Luque ◽  
...  
Keyword(s):  
Iron Oxide ◽  
Benzyl Alcohol ◽  
Iron Oxide Nanoparticles ◽  
Continuous Flow ◽  
Aerobic Oxidation ◽  
Oxide Nanoparticles ◽  
Oxidation Of Benzyl Alcohol ◽  
Supported Iron

Antimicrobial activity of citric acid functionalized iron oxide nanoparticles –Superparamagnetic effect

2020 ◽  
Vol 46 (8) ◽  
pp. 10942-10951 ◽  
Author(s):  
Sidra Khan ◽  
Zaheer H. Shah ◽  
Saira Riaz ◽  
Naveed Ahmad ◽  
Shumaila Islam ◽  
...  
Keyword(s):  
Antimicrobial Activity ◽  
Iron Oxide ◽  
Citric Acid ◽  
Iron Oxide Nanoparticles ◽  
Oxide Nanoparticles

Synthesis of iron oxide nanoparticles in a continuous flow spiral microreactor and Corning® advanced flow™ reactor

2018 ◽  
Vol 7 (1) ◽  
pp. 1-11 ◽  
Author(s):  
Prashant L. Suryawanshi ◽  
Shirish H. Sonawane ◽  
Bharat A. Bhanvase ◽  
Muthupandian Ashokkumar ◽  
Makarand S. Pimplapure ◽  
...  
Keyword(s):  
Particle Size ◽  
Iron Oxide ◽  
Iron Oxide Nanoparticles ◽  
Continuous Flow ◽  
Xrd Analysis ◽  
Resonance Spectroscopy ◽  
Oxide Nanoparticles ◽  
Flow Rates ◽  
Nanometer Size Range ◽  
Co Precipitation

AbstractIn the present work, synthesis of iron oxide nanoparticles (NPs) using continuous flow microreactor (MR) and advanced flow™ reactor (AFR™) has been investigated with evaluation of the efficacy of the two types of MRs. Effect of the different operating parameters on the characteristics of the obtained NPs has also been investigated. The synthesis of iron oxide NPs was based on the co-precipitation and reduction reactions using iron (III) nitrate precursor and sodium hydroxide as reducing agents. The iron oxide NPs were characterized using transmission electron microscopy (TEM), Fourier transform infrared spectroscopy, and X-ray diffraction (XRD) analysis. The mean particle size of the obtained NPs was less than 10 nm at all flow rates (over the range of 20−60 ml/h) in the case of spiral MR, while, in the case of AFR™, the particle size of NPs was below 20 nm with no specific trend observed with the operating flow rates. The XRD and TEM analyses of iron oxide NPs confirmed the crystalline nature and nanometer size range, respectively. Further, magnetic properties of the synthesized iron oxide NPs were studied using electron spin resonance spectroscopy; the resonance absorption peak shows theg-factor values as 2.055 and 2.034 corresponding to the magnetic fields of 319.28 and 322.59 mT for MR and AFR™, respectively.

Continuous Flow Preparation of Iron Oxide Nanoparticles Supported on Porous Silicates

ChemCatChem ◽  
2014 ◽  
Vol 7 (2) ◽  
pp. 276-282 ◽  
Author(s):  
Alfonso Yepez ◽  
Frank L. Y. Lam ◽  
Antonio A. Romero ◽  
C. Oliver Kappe ◽  
Rafael Luque
Keyword(s):  
Iron Oxide ◽  
Iron Oxide Nanoparticles ◽  
Continuous Flow ◽  
Oxide Nanoparticles

Effect of synthesis conditions on the properties of citric-acid coated iron oxide nanoparticles

2013 ◽  
Vol 110 ◽  
pp. 329-334 ◽  
Author(s):  
L. Li ◽  
K.Y. Mak ◽  
C.W. Leung ◽  
K.Y. Chan ◽  
W.K. Chan ◽  
...  
Keyword(s):  
Iron Oxide ◽  
Citric Acid ◽  
Iron Oxide Nanoparticles ◽  
Oxide Nanoparticles ◽  
Synthesis Conditions

scholarly journals Tuning Sizes, Morphologies, and Magnetic Properties of Monocore Versus Multicore Iron Oxide Nanoparticles through the Controlled Addition of Water in the Polyol Synthesis

2017 ◽  
Vol 56 (14) ◽  
pp. 8232-8243 ◽  
Author(s):  
Gauvin Hemery ◽  
Anthony C. Keyes ◽  
Eneko Garaio ◽  
Irati Rodrigo ◽  
Jose Angel Garcia ◽  
...  
Keyword(s):  
Magnetic Properties ◽  
Iron Oxide ◽  
Iron Oxide Nanoparticles ◽  
Polyol Synthesis ◽  
Oxide Nanoparticles

Magnetic Fixation of Dendron-Functionalized Iron Oxide Nanoparticles with Palladium for Continuous-Flow Suzuki Reactions

2016 ◽  
Vol 88 (9) ◽  
pp. 1338-1338 ◽  
Author(s):  
T. H. Rehm ◽  
C. Hofmann ◽  
P. Löb ◽  
Z. B. Shifrina ◽  
D. G. Morgan ◽  
...  
Keyword(s):  
Iron Oxide ◽  
Iron Oxide Nanoparticles ◽  
Continuous Flow ◽  
Oxide Nanoparticles ◽  
Suzuki Reactions
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