Preparation and characterization of periodic mesoporous organosilica terminally functionalized with fluorocarbon groups by a direct synthesis

2007 ◽  
Vol 44 (2) ◽  
pp. 105-110 ◽  
Author(s):  
Qi Wei ◽  
Li Liu ◽  
Zuo-Ren Nie ◽  
Hui-Qiao Chen ◽  
Jing-Xia Zou
Keyword(s):  
Direct Synthesis ◽  
Periodic Mesoporous Organosilica ◽  
Mesoporous Organosilica

Periodic Mesoporous Organosilica as a Multifunctional Nanodevice for Large-Scale Characterization of Membrane Proteins

2012 ◽  
Vol 84 (13) ◽  
pp. 5809-5815 ◽  
Author(s):  
Jinrui Gan ◽  
Jie Zhu ◽  
Guoquan Yan ◽  
Yun Liu ◽  
Pengyuan Yang ◽  
...  
Keyword(s):  
Membrane Proteins ◽  
Large Scale ◽  
Periodic Mesoporous Organosilica ◽  
Mesoporous Organosilica ◽  
Scale Characterization

Synthesis and characterization of rod-like periodic mesoporous organosilica with the 1,4-diureylenebenzene moieties

2007 ◽  
Vol 103 (1-3) ◽  
pp. 184-189 ◽  
Author(s):  
Junning Li ◽  
Tao Qi ◽  
Lina Wang ◽  
Ying Zhou ◽  
Changhou Liu ◽  
...  
Keyword(s):  
Synthesis And Characterization ◽  
Periodic Mesoporous Organosilica ◽  
Mesoporous Organosilica

Functionalization of periodic mesoporous organosilica with ureidopropyl groups by a direct synthesis method

2007 ◽  
Vol 101 (3) ◽  
pp. 381-387 ◽  
Author(s):  
Qi Wei ◽  
Li Liu ◽  
Zuo-Ren Nie ◽  
Hui-Qiao Chen ◽  
Yan-Li Wang ◽  
...  
Keyword(s):  
Direct Synthesis ◽  
Synthesis Method ◽  
Periodic Mesoporous Organosilica ◽  
Mesoporous Organosilica

scholarly journals Preparation and Characterization of Novel Mixed Periodic Mesoporous Organosilica Nanoparticles

Materials ◽  
2020 ◽  
Vol 13 (7) ◽  
pp. 1569
Author(s):  
Hao Li ◽  
Laurence Raehm ◽  
Clarence Charnay ◽  
Jean-Olivier Durand ◽  
Roser Pleixats
Keyword(s):  
Cetyltrimethylammonium Bromide ◽  
Sol Gel ◽  
X Ray Diffraction ◽  
Periodic Mesoporous Organosilica ◽  
X Ray ◽  
Surface Areas ◽  
Mesoporous Organosilica ◽  
Transmission Electron ◽  
Cp Mas Nmr

We report herein the preparation of mixed periodic mesoporous organosilica nanoparticles (E-Pn 75/25 and 90/10 PMO NPs) by sol-gel co-condensation of E-1,2-bis(triethoxysilyl)ethylene ((E)-BTSE or E) with previously synthesized disilylated tert-butyl 3,5-dialkoxybenzoates bearing either sulfide (precursor P1) or carbamate (precursor P2) functionalities in the linker. The syntheses were performed with cetyltrimethylammonium bromide (CTAB) as template in the presence of sodium hydroxide in water at 80 °C. The nanomaterials have been characterized by Transmission Electron Microscopy (TEM), nitrogen-sorption measurements (BET), Dynamic Light Scattering (DLS), zeta-potential, Thermogravimetric Analysis (TGA), FTIR, 13C CP MAS NMR and small angle X-ray diffraction (p-XRD). All the nanomaterials were obtained as mesoporous rodlike-shape nanoparticles. Remarkably, E-Pn 90/10 PMO NPs presented high specific surface areas ranging from 700 to 970 m2g−1, comparable or even higher than pure E PMO nanorods. Moreover, XRD analyses showed an organized porosity for E-P1 90/10 PMO NPs typical for a hexagonal 2D symmetry. The other materials showed a worm-like mesoporosity.

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