Influence of substrate on high-temperature behavior of copper film studied in situ by electron backscatter diffraction

2005 ◽  
Vol 34 (12) ◽  
pp. 1509-1520 ◽  
Author(s):  
Kabirkumar J. Mirpuri ◽  
Jerzy A. Szpunar
Keyword(s):  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
Copper Film ◽  
Temperature Behavior ◽  
High Temperature Behavior ◽  
Electron Backscatter ◽  
Influence Of Substrate ◽  
Backscatter Diffraction

High temperature behavior of Cu films studied in-situ by Electron Backscatter Diffraction

2004 ◽  
Vol 76 (1-4) ◽  
pp. 160-166 ◽  
Author(s):  
K. Mirpuri ◽  
H. Wendrock ◽  
S. Menzel ◽  
K. Wetzig ◽  
J. Szpunar
Keyword(s):  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
Temperature Behavior ◽  
Cu Films ◽  
High Temperature Behavior ◽  
Electron Backscatter ◽  
Backscatter Diffraction

"In Situ-Tracking” Observation of Stainless Steel Microstructural Development during Elevated Service Using EBSD and SEM

2007 ◽  
Vol 561-565 ◽  
pp. 2087-2090 ◽  
Author(s):  
Ya Ming Huang ◽  
Qiang Fu ◽  
Chun Xu Pan
Keyword(s):  
Stainless Steel ◽  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
Microstructural Development ◽  
Dislocation Model ◽  
Recrystallization Process ◽  
Novel Technique ◽  
Electron Backscatter ◽  
Backscatter Diffraction

Electron backscatter diffraction (EBSD) has been developed as a novel technique for characterizing crystallographic textures in recent years. The present paper proposes an “in-situ-tracking” approach using SEM and EBSD to examining the microstructural development and grain boundary variation of stainless steel during elevated 1200 °C service. The results revealed that in addition to the coarsened grains the fraction of low angle grain boundaries (LABG) became increased and flattened obviously during service. Comparing to the regular high temperature service (below 900 °C), the present “recovery and recrystallization” process was accelerated due to dislocation fastened movement and intensive interaction. However, the grain growth mechanism still meet the well-accepted dislocation model of subgrain combination.

scholarly journals Investigation of the α−γ−α Phase Transformation in Steel: High-Temperature In Situ EBSD Measurements

2008 ◽  
Vol 2008 ◽  
pp. 1-7 ◽  
Author(s):  
I. Lischewski ◽  
D. M. Kirch ◽  
A. Ziemons ◽  
G. Gottstein
Keyword(s):  
Phase Transformation ◽  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
Experimental Setup ◽  
Ebsd Data ◽  
Α Phase ◽  
Electron Backscatter ◽  
First Results ◽  
Backscatter Diffraction

A newly developed laser powered heating stage for commercial SEMs in combination with automated established electron backscatter diffraction (EBSD) data acquisition is presented. This novel experimental setup can be used to achieve more information about microstructure and orientation changes during grain growth, recrystallization, recovery, and phase transformations. First results on the α−γ−α phase transformation in steel within 886∘C–900∘C are presented.

scholarly journals Novel −75°C SEM cooling stage: application for martensitic transformation in steel

Microscopy ◽  
2020 ◽  
Author(s):  
Kaneaki Tsuzazki ◽  
Motomichi Koyama ◽  
Ryosuke Sasaki ◽  
Keiichiro Nakafuji ◽  
Kazushi Oie ◽  
...  
Keyword(s):  
Martensitic Transformation ◽  
Electron Backscatter Diffraction ◽  
Dislocation Slip ◽  
In Situ Observation ◽  
Contrast Imaging ◽  
Cooling Stage ◽  
Electron Channelling ◽  
Electron Backscatter ◽  
Backscatter Diffraction

Abstract Microstructural changes during the martensitic transformation from face-centred cubic (FCC) to body-centred cubic (BCC) in an Fe-31Ni alloy were observed by scanning electron microscopy (SEM) with a newly developed Peltier stage available at temperatures to  −75°C. Electron channelling contrast imaging (ECCI) was utilized for the in situ observation during cooling. Electron backscatter diffraction analysis at ambient temperature (20°C) after the transformation was performed for the crystallographic characterization. A uniform dislocation slip in the FCC matrix associated with the transformation was detected at −57°C. Gradual growth of a BCC martensite was recognized upon cooling from −57°C to −63°C.

scholarly journals High-temperature behavior of natural ferrierite: In-situ synchrotron X-ray powder diffraction study

2018 ◽  
Vol 103 (11) ◽  
pp. 1741-1748 ◽  
Author(s):  
Rossella Arletti ◽  
Riccardo Fantini ◽  
Carlotta Giacobbe ◽  
Reto Gieré ◽  
Giovanna Vezzalini ◽  
...  
Keyword(s):  
High Temperature ◽  
Diffraction Study ◽  
Powder Diffraction ◽  
Temperature Behavior ◽  
X Ray ◽  
High Temperature Behavior

In-situ Recrystallization Experiments Using Electron Backscatter Diffraction

2007 ◽  
Vol 13 (S02) ◽  
Author(s):  
D Prior ◽  
M Bestmann ◽  
S Piazolo ◽  
NC Seaton ◽  
DJ Tatham ◽  
...  
Keyword(s):  
Electron Backscatter Diffraction ◽  
Electron Backscatter ◽  
Backscatter Diffraction

Surface Crystallization of Cordierite from Glass Studied by High-Temperature X-ray Diffraction and Electron Backscatter Diffraction (EBSD)

2011 ◽  
Vol 11 (10) ◽  
pp. 4660-4666 ◽  
Author(s):  
Wolfgang Wisniewski ◽  
Carlos André Baptista ◽  
Matthias Müller ◽  
Günter Völksch ◽  
Christian Rüssel
Keyword(s):  
High Temperature ◽  
Electron Backscatter Diffraction ◽  
Surface Crystallization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Electron Backscatter ◽  
Backscatter Diffraction
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