Accuracy and precision of phase analysis in portland cement by Bogue, microscopic and X-ray diffraction methods

1982 ◽  
Vol 12 (3) ◽  
pp. 381-398 ◽  
Author(s):  
L.P. Aldridge
2018 ◽  
Vol 149 ◽  
pp. 01073
Author(s):  
K. Ben Addi ◽  
A. Diouri ◽  
N. Khachani ◽  
A. Boukhari

This paper investigates the mineralogical evolution of sulfoaluminate clinker elaborated from moroccan prime materials limestone, shale and phosphogypsum as a byproduct from phosphoric acid factories. The advantage of the production of this type of clinker is related to the low clinkerisation temperature which is known around 1250°C, and to less consumption quantity of limestone thus enabling less CO2 emissions during the decarbonation process compared to that of Portland cement. In this study we determine the stability conditions of belite sulfoaluminate clinker containing belite (C2S) ye’elimite (C4A3$) and ternesite (C5S2$). The hydration compounds of this clinker are also investigated. The monitoring of the synthesized and hydrated phases is performed by X-Ray Diffraction and Infrared spectroscopy. The results show the formation of ternesite at 800°C and the stabilization of clinker containing y’elminite, belite and ternesite at temperatures between 1100 and 1250°C.


1982 ◽  
pp. 237-244 ◽  
Author(s):  
T. M. Hare ◽  
J. C. Russ ◽  
M. J. Lanzo

2020 ◽  
Vol 20 (4) ◽  
pp. 205-223
Author(s):  
Fernanda Nepomuceno Costa ◽  
Daniel Véras Ribeiro ◽  
Cléber Marcos Ribeiro Dias

Abstract Efforts to reduce greenhouse gas emissions in the context of sustainable development have intensified, with the development of research aimed at the production of new materials and binders for construction. This article analyzes the influence of pellet geometry in the production of clinkers, with the incorporation of construction waste (CCW). Procedures adapted from the method proposed by Brazilian Portland Cement Association were adopted in studies of laboratory clinkers, in an attempt to simulate the stages of the industrial process. Pellets were prepared with the same formulation, however, with four different geometries: spherical, with diameters of 1 cm, 2 cm and 3 cm, with manual molding, and semi-spherical, with a diameter of 2 cm, using molds of PLA (polylactic acid) printed on a 3D printer to facilitate the molding of the clinkers in a standardized way. Clinkers were characterized mineralogically by x-ray diffraction (XRD) and the Rietveld method was used to quantify the phases. Variations in the quantities of the alite and belite phases were observed depending on the geometry of the pellets, although the same calcination conditions were used. This is probably due to the variation in the surface area (exposure area) and the gradients of the cooling rate.


Sign in / Sign up

Export Citation Format

Share Document