Determination of oxalic acid in urine by atomic absorption spectrophotometry

1976 ◽  
Vol 70 (1) ◽  
pp. 71-77 ◽  
Author(s):  
C. Koehl ◽  
J. Abecassis
Keyword(s):  
Oxalic Acid ◽  
Atomic Absorption ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Spectrophotometry

Routine Micromethod for Determination of Oxalic Acid in Urine by Atomic Absorption Spectrophotometry

1974 ◽  
Vol 20 (11) ◽  
pp. 1444-1445 ◽  
Author(s):  
R Menachè
Keyword(s):  
Oxalic Acid ◽  
Atomic Absorption ◽  
Calcium Ions ◽  
Atomic Absorption Spectrophotometry ◽  
Total Calcium ◽  
Absorption Spectrophotometry ◽  
The Difference

Abstract The method of Gitelson et al. was modified to a microscale procedure and adapted for atomic absorption spectrophotometry. Oxalic acid in urine is precipitated with excess of calcium ions at pH 5. The excess of calcium present in the supernate and the total calcium added and present in the urine at pH 2 are determined by atomic absorption spectrophotometry. The oxalic acid present in the precipitate is calculated indirectly from the difference between the two determinations of calcium. This method is useful for routine determination of urinary oxalic acid.

Determination of Minor Nutrients in Fertilizers by Atomic Absorption Spectrophotometry: Second Collaborative Study

1965 ◽  
Vol 48 (6) ◽  
pp. 1100-1103
Author(s):  
C H Mcbride
Keyword(s):  
Atomic Absorption ◽  
Collaborative Study ◽  
Atomic Absorption Spectrophotometry ◽  
Absorption Method ◽  
Atomic Absorption Method ◽  
Absorption Spectrophotometry ◽  
Minor Nutrients

Abstract The atomic absorption method studied last year was re-examined and extended to include calcium and sodium. The procedures were submitted to 16 collaborators for determination of Ca, Cu, Fe, Mg, Mn, Na, and Zn. Results for Ca and Na were discouraging; further study is recommended.

Comparison of Methods for Determining Biuret in Urea

1979 ◽  
Vol 62 (1) ◽  
pp. 153-159
Author(s):  
Luis F Corominas ◽  
Victor M Boy ◽  
Manuel Guijosa
Keyword(s):  
Atomic Absorption ◽  
Spectrophotometric Determination ◽  
Atomic Absorption Spectrophotometry ◽  
International Organization ◽  
Comparison Of Methods ◽  
Definite Advantage ◽  
Absorption Spectrophotometry ◽  
Alternative Procedures ◽  
Aoac Method

Abstract The official first action AOAC method for the spectrophotometric determination of biuret in urea, 2.072—2.074, was compared with official first action AOAC method 2.C01-2.C03 (atomic absorption spectrophotometry), 2 simplified versions of 2.072-2.074, and modified versions of 2 alternative procedures of the International Organization for Standardization. Three synthetic urea samples (0.3, 1.4, and 3.0% biuret) and 1 commercial urea sample (1.0% biuret) were analyzed. The methods proved to be equivalent and none showed a definite advantage over 2.072-2.074. The purification of biuret and the interference by ammonia are also discussed.

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