3D electron diffraction for structural characterization of nanomaterials

Author(s):  
Hongyi Xu
1996 ◽  
Vol 52 (6) ◽  
pp. 932-938 ◽  
Author(s):  
C. D. Ling ◽  
S. Schmid ◽  
J. G. Thompson ◽  
R. L. Withers ◽  
M. Sterns

Attempts to synthesize Sb-based analogues of the known Bi-based Aurivillius phase, Bi3TiNbO9, have led to the discovery of an isomorphous pair of a new type of layered intergrowth phase of general stoichiometry Sb3+x Nb3−x TiO14 and Sb3+x Ta3−x TiO14. Electron diffraction proved essential for the initial recognition and structural characterization of these phases. The structures of Sb3+x Nb3−x TiO14, x = 0.89, and Sb3+x Ta3−x TiO14, x = 1.26, are reported. The structures are described as ordered intergrowths of β-Sb2O4-type and Sb2O5-type structures, with NbV/TaV substituting for SbV in the former and NbV/TaV/TiIV substituting for SbV in the latter.


2010 ◽  
Vol 50 (3) ◽  
pp. 385-409 ◽  
Author(s):  
Ute Kolb ◽  
Tatiana E. Gorelik ◽  
Enrico Mugnaioli ◽  
Andrew Stewart

2007 ◽  
Vol 101 (5) ◽  
pp. 056106 ◽  
Author(s):  
J. Coraux ◽  
V. Favre-Nicolin ◽  
H. Renevier ◽  
M. G. Proietti ◽  
B. Amstatt ◽  
...  

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