scholarly journals Preparation and characterization of mesoporous activated carbons from waste watermelon rind by using the chemical activation method with zinc chloride

2019 ◽  
Vol 12 (8) ◽  
pp. 3621-3627 ◽  
Author(s):  
Osman Üner ◽  
Ünal Geçgel ◽  
Yüksel Bayrak
2015 ◽  
Vol 74 (11) ◽  
Author(s):  
Riry Wirasnita ◽  
Tony Hadibarata ◽  
Abdull Rahim Mohd Yusoff ◽  
Zainab Mat Lazim

An oil palm empty fruit bunch-derived activated carbon has been successfully produced by chemical activation with zinc chloride and without chemical activation. The preparation was conducted in the tube furnace at 500oC for 1 h. The surface structure and active sites of activated carbons were characterized by means of Fourier transform infrared spectrometry and field emission scanning electron microscopy. The proximate analysis including moisture content, ash content, bulk density, pH, and pH at zero charge was conducted to identify the psychochemical properties of the adsorbent. The results showed that the zinc chloride-activated carbon has better characteristics compared to the carbon without chemical activation.  


2018 ◽  
Vol 23 (4) ◽  
pp. 1-15 ◽  
Author(s):  
Kuete Tiotsop Idris-Hermann ◽  
Tchuifon Tchuifon Donald Raoul ◽  
Doungmo Giscard ◽  
Anagho Solomon Gabche

2010 ◽  
Vol 7 (2) ◽  
pp. 531-539 ◽  
Author(s):  
Diana Paola Vargas-Delgadillo ◽  
Liliana Giraldo ◽  
Juan Carlos Moreno-Piraján

A series of different activated carbons of both honeycomb and disc type were prepared by chemical activation of coconut shells with zinc chloride at different concentrations, without the use of a binder. The structures were characterized by N2adsorption at 77 K and scanning electron microscopy (SEM), and also some samples were characterized by immersion calorimetry in benzene. These were subsequently used in the adsorption of phenol in aqueous solution. The experimental results indicat that activation with zinc chloride produced a large development of microporosity with a micropore volume of 0.38 to 0.79 cm3g-1, BET area between 725 and 1523 m2g-1and the capacity to adsorb phenol. In addition, the BET and Langmuir models were applied to isotherm data.


2018 ◽  
Author(s):  
Wahyuningsih ◽  
Zainal Abidin ◽  
Mohamad Endy Yulianto ◽  
Indah Hartati ◽  
Eflita Yohana

2021 ◽  
Vol 2049 (1) ◽  
pp. 012067
Author(s):  
Rakhmawati Farma ◽  
Ramadani Putri Anakis ◽  
Irma Apriyani

Abstract Biomass converted into activated carbon (AC) by using physical activation method can form micro-meso pore structure and maintain the interconnected natural pore network of biomass. AC is prepared from the biomass of Parsea Americana seeds (PAS) through a process of pre-carbonization, chemical activation, carbonization and physical activation which is activated at temperatures of 700°C, 800°C, and 900°C. Characterization of physical properties of AC electrodes consisted of X-ray diffraction, Scanning Electron Microscope-Energy Dispersive X-ray and characterization of electrochemical properties of supercapacitor cells using Cyclic Voltametry. The results showed that the microstructure of the AC electrode has a semicrystalline structure characterized by the presence of two sloping peaks at an angle of 2θ around 24° and 44° which corresponded to the hkl (002) and (100) planes, where the lowest Lc value was produced by the PAS-900 sample. The PAS-900 sample had aggregates or lumps with smaller size in small amounts in the presence of micro-mesopores and had the highest carbon content of 94.50% with the highest capacitance value of 203.12 F/g. The temperature of 900°C is the best activation temperature in the process of manufacture AC electrodes from Parsea Americana seeds biomass for supercapacitor cell applications.


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