Optimization of experimental conditions based on the Taguchi robust design for the formation of nano-sized silver particles by chemical reduction method

2004 ◽  
Vol 104 (1-3) ◽  
pp. 55-61 ◽  
Author(s):  
Ki Do Kim ◽  
Dae Nam Han ◽  
Hee Taik Kim
Keyword(s):  
Robust Design ◽  
Reduction Method ◽  
Chemical Reduction ◽  
Silver Particles ◽  
Chemical Reduction Method ◽  
Experimental Conditions ◽  
Taguchi Robust Design ◽  
Optimization Of Experimental Conditions

Effect of Surfactant on the Morphology of Silver Nanoparticles

2007 ◽  
Vol 124-126 ◽  
pp. 1205-1208 ◽  
Author(s):  
Keun Ju Park ◽  
Dong Seok Seo ◽  
Woo Yang Jang ◽  
Jong Kook Lee
Keyword(s):  
Silver Nanoparticles ◽  
Ascorbic Acid ◽  
Low Temperature ◽  
Reduction Method ◽  
Chemical Reduction ◽  
Sodium Dodecyl ◽  
Capping Agent ◽  
Silver Particles ◽  
Chemical Reduction Method ◽  
20 Nm

Nano-sized silver particles are considered to apply a silver paste for electrode because of its high conductivity on sintering at low temperature. In this study, silver nanoparticles as seeds were prepared by chemical reduction method with capping agent. Silver particles were prepared using SDS (Sodium dodecyl sulfate) as a surfactant and silver nanoparticles as seeds and reacted with ascorbic acid as a reduction agent. The silver seeds with 10-20 nm in size with uniform distribution were formed and the size and shape of silver particles were strongly dependent on the concentration of surfactant.

scholarly journals OPTIMIZATION OF THE EXPERIMENTAL CONDITIONS IN SYNTHESIS OF Au NPs USING PREYSSLER HETEROPOLYACID BASED ON THE TAGUCHI ROBUST DESIGN

NANO ◽  
2012 ◽  
Vol 07 (01) ◽  
pp. 1250002 ◽  
Author(s):  
ALI AYATI ◽  
ALI AHMADPOUR ◽  
FATEMEH F. BAMOHARRAM ◽  
MAJID M. HERAVI ◽  
HAMED RASHIDI
Keyword(s):  
Gold Nanoparticles ◽  
Robust Design ◽  
Design Method ◽  
Irradiation Time ◽  
Chemical Reduction ◽  
Experimental Conditions ◽  
Acid Amount ◽  
Vis Spectroscopy ◽  
Robust Design Method ◽  
Taguchi Robust Design

Preparation of gold nanoparticles by chemical reduction method using Preyssler heteropolyacid was investigated. The experimental conditions have been optimized using Taguchi robust design method with L9 orthogonal array. Particle size of the gold nanoparticles was considered as the property in the optimization. Amounts of Preyssler heteropolyacid, pH and irradiation time were selected as the main parameters. The result of Taguchi analysis has shown that in this process, the preyssler acid amount is the most influencing parameter on the size of gold nanoparticle. Also, the effects of different parameters are in order to: Preyssler acid amount > pH > irradiation time (negligible). This method showed that decreasing Preyssler amount and increasing pH of solution lead to formation of smaller nanoparticles. Finally, the prepared nanoparticles at optimum condition with a size of about 6.42 were characterized by using Dynamic Light Scattering (DLS) method, transmission electron microscopy (TEM), and UV-Vis spectroscopy.

Antimicrobial Activity of Silver Nanoparticles Prepared Under an Ultrasonic Field

2011 ◽  
Vol 4 (3) ◽  
pp. 1491-1496
Author(s):  
Umadevi M ◽  
Rani T ◽  
Balakrishnan T ◽  
Ramanibai R
Keyword(s):  
Escherichia Coli ◽  
Antimicrobial Activity ◽  
Silver Nanoparticles ◽  
Reduction Method ◽  
Therapeutic Potential ◽  
Chemical Reduction ◽  
Ultrasonic Field ◽  
Great Promise ◽  
Chemical Reduction Method ◽  
E Coli

Nanotechnology has great promise for improving the therapeutic potential of medicinal molecules and related agents. In this study, silver nanoparticles of different sizes were synthesized in an ultrasonic field using the chemical reduction method with sodium borohydride as a reducing agent. The size effect of silver nanoparticles on antimicrobial activity were tested against the microorganisms Staphylococcus aureus (MTCC No. 96), Bacillus subtilis (MTCC No. 441), Streptococcus mutans (MTCC No. 497), Escherichia coli (MTCC No. 739) and Pseudomonas aeruginosa (MTCC No. 1934). The results shows that B. subtilis, and E. coli were more sensitive to silver nanoparticles and its size, indicating the superior antimicrobial efficacy of silver nanoparticles. 

scholarly journals Synthesis of Cu core Ag shell nanoparticles using chemical reduction method

2015 ◽  
Vol 6 (2) ◽  
pp. 025018 ◽  
Author(s):  
Dung Chinh Trinh ◽  
Thi My Dung Dang ◽  
Kim Khanh Huynh ◽  
Eric Fribourg-Blanc ◽  
Mau Chien Dang
Keyword(s):  
Reduction Method ◽  
Chemical Reduction ◽  
Chemical Reduction Method ◽  
Shell Nanoparticles
Sign in / Sign up

Export Citation Format

Share Document