Monitoring of cocrystallization of ethenzamide–saccharin: Insight into kinetic process by in situ Raman spectroscopy

2016 ◽  
Vol 109 ◽  
pp. 249-257 ◽  
Author(s):  
Yao Tong ◽  
Peng Zhang ◽  
Leping Dang ◽  
Hongyuan Wei
2017 ◽  
Vol 13 ◽  
pp. 2160-2168 ◽  
Author(s):  
Patrick A Julien ◽  
Ivani Malvestiti ◽  
Tomislav Friščić

We provide the first in situ and real-time study of the effect of milling frequency on the course of a mechanochemical organic reaction conducted using a vibratory shaker (mixer) ball mill. The use of in situ Raman spectroscopy for real-time monitoring of the mechanochemical synthesis of a 2,3-diphenylquinoxaline derivative revealed a pronounced dependence of chemical reactivity on small variations in milling frequency. In particular, in situ measurements revealed the establishment of two different regimes of reaction kinetics at different frequencies, providing tentative insight into processes of mechanical activation in organic mechanochemical synthesis.


Polymers ◽  
2018 ◽  
Vol 10 (4) ◽  
pp. 416 ◽  
Author(s):  
Krzysztof Bogdanowicz ◽  
Domenico Pirone ◽  
Judit Prats-Reig ◽  
Veronica Ambrogi ◽  
José Reina ◽  
...  

2020 ◽  
Vol 20 (10) ◽  
pp. 6604-6609
Author(s):  
Shanshan Liu ◽  
Guochun Zhang ◽  
Kai Feng ◽  
Yanyang Han ◽  
Tao He ◽  
...  

Carbon ◽  
2021 ◽  
Vol 177 ◽  
pp. 428
Author(s):  
Xiaoqin Cheng ◽  
Huijun Li ◽  
Zhenxin Zhao ◽  
Yong-zhen Wang ◽  
Xiaomin Wang

1991 ◽  
Vol 62 (7) ◽  
pp. 1743-1745 ◽  
Author(s):  
F. Spinella ◽  
G. A. Baratta ◽  
G. Strazzulla

Langmuir ◽  
2021 ◽  
Vol 37 (4) ◽  
pp. 1365-1371
Author(s):  
Sergei V. German ◽  
Gleb S. Budylin ◽  
Evgeny A. Shirshin ◽  
Dmitry A. Gorin

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