A simple and rapid method for the determination of lead dioxide in minium by headspace gas chromatographic technique

2020 ◽  
Vol 1617 ◽  
pp. 460832
Author(s):  
Wei-Qi Xie ◽  
Yi-Xian Gong ◽  
Shi-Wen Huang ◽  
Kong-Xian Yu
Keyword(s):  
Rapid Method ◽  
Lead Dioxide ◽  
Chromatographic Technique ◽  
Headspace Gas

Gas Chromatographic Method for Determination of Dimethylamine, Trimethylamine, and Trimethylamine Oxide in Fish-Meat Frankfurters

1991 ◽  
Vol 74 (2) ◽  
pp. 400-403
Author(s):  
Walter Fiddler ◽  
Robert C Doerr ◽  
Robert A Gates
Keyword(s):  
Atlantic Menhaden ◽  
Chromatographic Technique ◽  
Acid Extraction ◽  
Fish Meat ◽  
Flame Ionization ◽  
Trimethylamine Oxide ◽  
Headspace Gas ◽  
Gas Chromatographic Method ◽  
Gas Tight

Abstract A method Is described for analysis of minced fish-meat and surlmi-meat frankfurters for dimethylamine (DMA), trimethyiamine (TMA), and trimethyiamine oxide (TMAO) using a headspace-gas chromatographic technique. After simple acid extraction and addition of NaOH, the headspace was directly Injected Into a gas chromatograph by a gas-tight syringe. DMA and TMA were separated on a Chromosorb 103 column and detected by a flame Ionization detector. TMAO was measured as TMA after Zn reduction. Repeatability of the method for DMA, TMA, and TMAO was 6.6,1.0, and 18.8 ppm, respectively. The method was applicable to Alaska pollock-meat and Atlantic menhaden-meat frankfurters, unwashed, and washed mince and surlml.

Determination of the softening point of rosin by a simple and automated headspace gas chromatographic technique

2018 ◽  
Vol 41 (17) ◽  
pp. 3411-3414
Author(s):  
Yi Dai ◽  
Zhen-Hua Yu ◽  
Jian-Bo Zhan ◽  
Bao-Shan Yue ◽  
Jiao Xie ◽  
...  
Keyword(s):  
Softening Point ◽  
Chromatographic Technique ◽  
Headspace Gas

High-throughput determination of the organic matter content in soil and municipal sludge by headspace gas chromatography

2019 ◽  
Vol 11 (47) ◽  
pp. 5963-5968
Author(s):  
Xiaojie Tu ◽  
Zhanbo Hu ◽  
Ting Zhao ◽  
Xin-Sheng Chai ◽  
Jie Wang ◽  
...  
Keyword(s):  
Organic Matter ◽  
Acidic Medium ◽  
Rapid Determination ◽  
Organic Matter Content ◽  
Matter Content ◽  
Chromatographic Technique ◽  
Headspace Gas Chromatography ◽  
Municipal Sludge ◽  
Headspace Gas

This paper reports on a new headspace gas chromatographic technique for rapid determination of organic matter (OM) in soil and municipal sludge samples, based on a redox reaction, i.e., converting OM into CO2 by dichromate at an acidic medium.

Quantification of the amine value in aliphatic amine epoxy hardeners by using a reaction-based headspace gas chromatographic technique

2017 ◽  
Vol 9 (16) ◽  
pp. 2440-2444 ◽  
Author(s):  
Wei-Qi Xie ◽  
Yi-Xian Gong ◽  
Kong-Xian Yu
Keyword(s):  
Aliphatic Amine ◽  
Chromatographic Technique ◽  
Headspace Gas

This work investigates a reaction-based and solvent-assisted HS-GC method for the determination of the amine value in aliphatic amine epoxy hardeners.

Quantitative determination of the oleophobicity of food packaging paper using headspace gas chromatographic technique

2021 ◽  
Vol 34 (5) ◽  
pp. 297-302
Author(s):  
Yi Dai ◽  
Zhen‐Hua Yu ◽  
Hao Wang ◽  
Jian‐Bo Zhan ◽  
Jiao Xie ◽  
...  
Keyword(s):  
Quantitative Determination ◽  
Food Packaging ◽  
Chromatographic Technique ◽  
Headspace Gas ◽  
Packaging Paper

Rapid Screening Method for the Determination of Organochlorine Pesticide Residues in Wheat by Electron Capture Gas Chromatography

1972 ◽  
Vol 55 (4) ◽  
pp. 794-799
Author(s):  
Iser Levi ◽  
P B Mazur ◽  
T W Nowicki
Keyword(s):  
Rapid Method ◽  
Organochlorine Pesticide ◽  
Electron Capture ◽  
Pesticide Residues ◽  
Screening Method ◽  
Rapid Screening ◽  
Chromatographic Technique ◽  
Organochlorine Pesticide Residues ◽  
Rapid Screening Method

Abstract A rapid screening method, employing a gas chromatographic technique with electron capture detection, has been developed for t h e analysis of organochlorine pesticide residues in hard red spring wheat. Ground wheat is extracted by ball-milling with an ethyl etherhexane (3 + 97) extractant. After filtration, the extract is cleaned up on a partially deactivated Florisil column, using a single eluting system, ethyl ether-hexane (1 + 99). The eluate i s concentrated before gas chromatographic analysis. Sixteen organochlorine pesticide chemicals were recovered in excess of 80% from wheat samples fortified at 0.010 and 0.200 ppm. Organochlorine pesticide residues were recovered by the rapid method from 18 samples with field-incurred residues as efficiently as by t he Bertuzzi et al. method. Organochlorine pesticide residues were also recovered by t h e rapid method from 4 samples with field-incurred residues and from 2 wheat samples, spiked at 0.500 ppm as efficiently as by the total extraction method of Mumma et al. The rapid method offers a savings in time and solvents over.the Bertuzzi et al. method for the determination of organochlorine pesticide residues in wheat.

Efficient Determination of Specific Surface Area of Shale Samples Using a Tracer-Based Headspace Gas Chromatographic Technique

2016 ◽  
Vol 89 (1) ◽  
pp. 974-979 ◽  
Author(s):  
Liang He ◽  
Teng-Fei Li ◽  
Xin-Sheng Chai ◽  
Hui Tian ◽  
Xian-Ming Xiao ◽  
...  
Keyword(s):  
Specific Surface ◽  
Surface Area ◽  
Specific Surface Area ◽  
Chromatographic Technique ◽  
Headspace Gas
Sign in / Sign up

Export Citation Format

Share Document