The mechanism of abnormal grain growth in polycrystalline diamond during high pressure-high temperature sintering

2004 ◽  
Vol 13 (3) ◽  
pp. 488-494 ◽  
Author(s):  
Taek-Jung Shin ◽  
Jeang-Ook Oh ◽  
Kyu Hwan Oh ◽  
Dong Nyung Lee
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Grain Growth ◽  
Polycrystalline Diamond ◽  
Abnormal Grain Growth ◽  
High Pressure High Temperature

Niobium as a new binder for polycrystalline diamond (PCD) sintered via High Pressure-High Temperature (HPHT)

2020 ◽  
Vol 90 ◽  
pp. 105234 ◽  
Author(s):  
Diego Pires Gurgel ◽  
Mayara Adrielly Leal de Oliveira Rodrigues ◽  
Meysam Mashhadikarimi ◽  
Lucas Pires de Paiva Barreto ◽  
Marcello Filgueira ◽  
...  
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Polycrystalline Diamond ◽  
High Pressure High Temperature

Microstructural Study of Diamond Deformed Under High Pressure and Temperature

1985 ◽  
Vol 43 ◽  
pp. 230-231
Author(s):  
E. F. Koch
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Lattice Structure ◽  
Diamond Particle ◽  
Polycrystalline Diamond ◽  
Sintering Process ◽  
Ion Milling ◽  
Sintered Compact ◽  
Transmission Electron ◽  
High Pressure Sintering

Because of the extremely rigid lattice structure of diamond, generating new dislocations or moving existing dislocations in diamond by applying mechanical stress at ambient temperature is very difficult. Analysis of portions of diamonds deformed under bending stress at elevated temperature has shown that diamond deforms plastically under suitable conditions and that its primary slip systems are on the ﹛111﹜ planes. Plastic deformation in diamond is more commonly observed during the high temperature - high pressure sintering process used to make diamond compacts. The pressure and temperature conditions in the sintering presses are sufficiently high that many diamond grains in the sintered compact show deformed microtructures.In this report commercially available polycrystalline diamond discs for rock cutting applications were analyzed to study the deformation substructures in the diamond grains using transmission electron microscopy. An individual diamond particle can be plastically deformed in a high pressure apparatus at high temperature, but it is nearly impossible to prepare such a particle for TEM observation, since any medium in which the diamond is mounted wears away faster than the diamond during ion milling and the diamond is lost.

scholarly journals High-pressure synthesis and crystal structure of the mixed-cation borate Ga4In4B15O33(OH)3

2019 ◽  
Vol 74 (4) ◽  
pp. 357-363
Author(s):  
Daniela Vitzthum ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Mixed Cation ◽  
High Pressure High Temperature ◽  
Pressure Synthesis

AbstractThe mixed cation triel borate Ga4In4B15O33(OH)3 was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined via single-crystal X-ray diffraction data. Ga4In4B15O33(OH)3 crystallizes in the tetragonal space group I41/a (origin choice 2) with the lattice parameters a = 11.382(2), c = 15.244(2) Å, and V = 1974.9(4) Å3. The structure of the quaternary triel borate consists of a complex network of BO4 tetrahedra, edge-sharing InO6 octahedra in dinuclear units, and very dense edge-sharing GaO6 octahedra in tetranuclear units.

Iodine-mediated high-pressure high-temperature carbonization of hydrocarbons and synthesis of nanodiamonds

2021 ◽  
Vol 137 ◽  
pp. 111189
Author(s):  
E.A. Ekimov ◽  
K.M. Kondrina ◽  
I.P. Zibrov ◽  
S.G. Lyapin ◽  
M.V. Lovygin ◽  
...  
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
High Pressure High Temperature

scholarly journals Multianvil High-Pressure/High-Temperature Synthesis and Characterization of multiferroic HP-Co3TeO6

2021 ◽  
Author(s):  
Gunter Heymann ◽  
Elisabeth Selb ◽  
Toni Buttlar ◽  
Oliver Janka ◽  
Martina Tribus ◽  
...  
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Type Structure ◽  
Synthesis And Characterization ◽  
Temperature Synthesis ◽  
Space Group ◽  
Crystal System ◽  
High Temperature Synthesis ◽  
High Pressure High Temperature

By high-pressure/high-temperature multianvil synthesis a new high-pressure (HP) phase of Co3TeO6 was obtained. The compound crystallizes in the acentric trigonal crystal system of the Ni3TeO6-type structure with space group R3...

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