Rapid ion-pair liquid chromatographic method for the determination of fenbendazole marker residue in fermented dairy products

2017 ◽  
Vol 221 ◽  
pp. 884-890 ◽  
Author(s):  
Venetia I. Vousdouka ◽  
Elias P. Papapanagiotou ◽  
Apostolos S. Angelidis ◽  
Dimitrios J. Fletouris
Keyword(s):  
Dairy Products ◽  
Chromatographic Method ◽  
Ion Pair ◽  
Liquid Chromatographic Method ◽  
Fermented Dairy Products ◽  
Fermented Dairy ◽  
Liquid Chromatographic

Rapid ion–pair liquid chromatographic method for the determination of fenbendazole in cows' milk

The Analyst ◽  
1994 ◽  
Vol 119 (12) ◽  
pp. 2801-2804 ◽  
Author(s):  
Dimitrios J. Fletouris ◽  
Nickos A. Botsoglou ◽  
Ioannis E. Psomas ◽  
Antonios I. Mantis
Keyword(s):  
Chromatographic Method ◽  
Ion Pair ◽  
Liquid Chromatographic Method ◽  
Liquid Chromatographic

scholarly journals Determination of Apramycin in Swine Kidney Tissue by Liquid Chromatography with Fluorescence Detection

1998 ◽  
Vol 81 (6) ◽  
pp. 1141-1146 ◽  
Author(s):  
Daniel J Sweeney ◽  
Mark R Coleman
Keyword(s):  
Chromatographic Method ◽  
Kidney Tissue ◽  
Ion Pair ◽  
Fluorescence Detector ◽  
Coefficients Of Variation ◽  
Liquid Chromatographic Method ◽  
Liquid Chromatographic ◽  
Swine Kidney ◽  
Injection Procedure

Abstract A liquid chromatographic method for determining apramycin in swine kidney tissue is described. Apramycin is extracted from tissue with basic methanol and purified by ion-pair extraction. By using an automated derivatization and injection procedure, the purified extract is derivatized with ophthaldehyde, separated on a C18 column, and detected with a fluorescence detector. For fortified kidney samples, between-run coefficients of variation ranged from 4.8 to 7.1 % at 1.00 ppm and from 9.6 to 14.3% at 0.50 ppm. Recoveries ranged from 76 to 86%. Standard curves were linear over the range 10-100 ng/mL.

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