A catholically pre-treated low cost screen-printed carbon electrode surface for metal compounds electrocatalyst like hydrogen evolution activity

2019 ◽  
Vol 839 ◽  
pp. 59-66 ◽  
Author(s):  
Yu-Ju Chen ◽  
Ting-Hao Yang ◽  
Jen-Lin Chang ◽  
Wan-Ling Cheng ◽  
Annamalai Senthil Kumar ◽  
...  
2012 ◽  
Vol 571 ◽  
pp. 56-59
Author(s):  
Yu Fang Sha ◽  
Mei Zhao ◽  
Ming Quan Yang ◽  
Hai Xin Bai ◽  
Man Zhao

Biological multilayer films of redox polymer and horseradish peroxidase (HRP) were successfully assembled on a screen-printed carbon electrode using layer-by-layer (LBL) assembled method based on the electrostatic interaction. The screen-printed carbon electrode surface was modified by the positively charged redox polymer, and the negatively charged HRP by LBL method.


Author(s):  
Nattida Rongwaree ◽  
Tongchatra Watcharawittayakul ◽  
Cholthisa Sooksamphanwong ◽  
Phichamon Sakdarat ◽  
Chanchana Thanachayanont ◽  
...  

2012 ◽  
Vol 571 ◽  
pp. 538-541
Author(s):  
Yu Fang Sha ◽  
Mei Zhao ◽  
Fei Guo ◽  
Jun Xie ◽  
Wei Han

Improvement of sensitivity of electrochemical sandwich enzyme immunoassay has been achieved by electrodepositing redox polymer on screen-printed carbon electrode surface, on which sandwich complex were formed.


Linalool is a very important flavouring compound found in plants which is used in food and beverages. Linalool has been traditionally detected by analytical instruments such as gas chromatography (GC) coupled with mass spectroscopy(MS) which are not suitable for routine tests. For fast and low cost detection of chemical compounds electrochemial sensors are most suitable. Screen printed carbon electrode (SPCE) is one of the most popular and low cost device used for detection of chemical compounds. In this article we present the detection of linalool using a low cost preannodized commercial screen printed carbon electrode (SPCE). Traditionally electrochemical sensors are used in two terminal mode, however three terminal analysis of electrochemical sensors are found to be more rationale and accurate. In this paper we have analyzed detection of linalool by an advanced three terminal analysis. First we have performed cyclic voltammetry(CV) of the SPCE which showed clear oxidation peaks at different concentration of linalool. The input-output data of the CV has been used for analysis of the impedance of the SPCE.The impedance model of the SPCE was estimated by autoregressive moving average with exogenous inputs(ARMAX) modelling technique using the CV data. The three terminal impedance fitting revealed the values of electrical parameters and the parasitic elements at different linalool concentration. The stability limits of the SPCE was also determined from the pole-zero and Nyquist plots of the estimated models. Impedance behaviour to frequency of the SPCE was further analyzed by impedance plot( 𝒁 vs −𝒁 ′ ) from which we are able to relate the CV scan rate to the impedance of the SPCE. Finally the sensitivity and repeatability of the SPCE was determined using a measurement circuit.


Materials ◽  
2020 ◽  
Vol 13 (14) ◽  
pp. 3168
Author(s):  
Suhainie Ismail ◽  
Nor Azah Yusof ◽  
Jaafar Abdullah ◽  
Siti Fatimah Abd Rahman

Arsenic poisoning in the environment can cause severe effects on human health, hence detection is crucial. An electrochemical-based portable assessment of arsenic contamination is the ability to identify arsenite (As(III)). To achieve this, a low-cost electroanalytical assay for the detection of As(III) utilizing a silica nanoparticles (SiNPs)-modified screen-printed carbon electrode (SPCE) was developed. The morphological and elemental analysis of functionalized SiNPs and a SiNPs/SPCE-modified sensor was studied using field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), energy dispersive X-ray spectroscopy (EDX), and Fourier transform infrared spectroscopy (FTIR). The electrochemical responses towards arsenic detection were measured using the cyclic voltammetry (CV) and linear sweep anodic stripping voltammetry (LSASV) techniques. Under optimized conditions, the anodic peak current was proportional to the As(III) concentration over a wide linear range of 5 to 30 µg/L, with a detection limit of 6.2 µg/L. The suggested approach was effectively valid for the testing of As(III) found within the real water samples with good reproducibility and stability.


2021 ◽  
pp. 130574
Author(s):  
P.E. Resmi ◽  
Jeethu Raveendran ◽  
P.V. Suneesh ◽  
T. Ramanchandran ◽  
Bipin G Nair ◽  
...  

2014 ◽  
Vol 447 ◽  
pp. 162-168 ◽  
Author(s):  
Nicolaj Cruys-Bagger ◽  
Hirosuke Tatsumi ◽  
Kim Borch ◽  
Peter Westh

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