The present paper focuses the modelling and the simulation of a direct thixoextrusion test achieved on C38 semi-solid steel. Many parameters related to thermal, mechanical, material features are involved but are currently unknown. Consequently to validate the modelling and the simulation, it is important to get various experimental informations during the test and to correlate them with simulated results. In a previous paper (Becker et al, 2008), the force-displacement curve, the temperature within the die, the macro and micro structure obtained for different process parameters during thixoextrusion of C38 were investigated. In this work, those results are correlated to those obtained by simulations of the processing. The simulations were performed using the commercial software Forge®. The thermal modelling is based on the heat equation and the thermal boundary conditions involving the heat losses, the thermal conduction within the semi-solid slug and the die and the plastic dissipation as heat source. The latent heat associated to the liquid-solid phase transformation is not considered here. The constitutive equation of the material is given by a multi-scale modelling based on micromechanics and homogenization techniques, labelled as micro-macro modelling (Favier et al, 2009). Friction is modelled using the usual modified Tresca equation. The parameters of the model are determined (i) using literature results and (ii) to match various experimental measurements obtained during the test and described in Becker et al (2008) such as the die temperature during the test and the load-displacement curve. Comparisons between experimental and simulated reveal the presence of complex temperature field and the presence of zones having very low viscosities. These zones contribute actively to the semi-solid material flow.
High speed DSC (hyper-DSC) as a tool to measure the solubility of a drug within a solid or semi-solid matrix
