Investigation on size dependent structural and magnetic behavior of nickel ferrite nanoparticles prepared by sol–gel and hydrothermal methods

2009 ◽  
Vol 118 (1) ◽  
pp. 174-180 ◽  
Author(s):  
Manish Srivastava ◽  
S. Chaubey ◽  
Animesh K. Ojha
2017 ◽  
Vol 35 (1) ◽  
pp. 58-65 ◽  
Author(s):  
Ayaz Arif Khan ◽  
M. Javed ◽  
A. Rauf Khan ◽  
Yousaf Iqbal ◽  
Asif Majeed ◽  
...  

AbstractNanocrystalline NiFe2O4 particles were prepared by conventional sol-gel, citrate-nitrate sol-gel combustion and co-precipitation methods. The synthesized samples were annealed at 1000 °C for two hours and structural, chemical, morphological, optical and magnetic properties of nickel ferrite were investigated. The structural properties were investigated by X-ray diffraction (XRD) technique which confirmed the formation of single phase NiFe2O4 particles derived by the three methods. The chemical properties were analyzed by Fourier transform infrared (FT-IR) spectroscopy which confirmed the corresponding vibration modes in the samples. The optical properties were studied by UV-Vis spectroscopy. The morphological study of the as-synthesized samples was carried out by scanning electron microscopy (SEM). SEM images showed the agglomerated nanoparticles of NiFe2O4. The magnetic properties were investigated by vibrating sample magnetometer (VSM), which showed that the calcined samples exhibited typical magnetic behavior.


2015 ◽  
Vol 2015 ◽  
pp. 1-7 ◽  
Author(s):  
I. G. Blanco-Esqueda ◽  
G. Ortega-Zarzosa ◽  
J. R. Martínez ◽  
A. L. Guerrero

Magnetic composites with silver nanoparticles bonded to their surface were successfully prepared using a simple chemical method. By means of a sol-gel technique, nickel ferrite nanoparticles have been prepared and coated with silica to control and avoid their magnetic agglomeration. The structural and magnetic properties of the nanoparticles were studied in function of the annealing temperature. Then, silver nanoparticles were incorporated by hydrolysis-condensation of tetraethyl orthosilicate, which contains silver nitrate on the surface of the nickel ferrite-SiO2core/shell. Samples were characterized using X-ray diffraction, IR spectroscopy, SEM, and magnetometry. Results show that the silica covered the nickel ferrite nanoparticles and the silver nanoparticles remain stable in the surface of the composite.


2014 ◽  
Vol 70 (3) ◽  
pp. 400-404 ◽  
Author(s):  
M. Penchal Reddy ◽  
W. Madhuri ◽  
K. Sadhana ◽  
I. G. Kim ◽  
K. N. Hui ◽  
...  

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