Simultaneous determination of human pharmaceuticals in water samples by solid phase extraction and HPLC with UV-fluorescence detection

2013 ◽  
Vol 107 ◽  
pp. 165-171 ◽  
Author(s):  
Luisa Patrolecco ◽  
Nicoletta Ademollo ◽  
Paola Grenni ◽  
Antonella Tolomei ◽  
Anna Barra Caracciolo ◽  
...  
Keyword(s):  
Solid Phase Extraction ◽  
Simultaneous Determination ◽  
Fluorescence Detection ◽  
Water Samples ◽  
Solid Phase ◽  
Phase Extraction ◽  
Uv Fluorescence

scholarly journals Development and optimization of a method for the determination of simazine, atrazine and propazine using solid-phase extraction and HPLC/GC

2001 ◽  
Vol 66 (3) ◽  
pp. 199-204 ◽  
Author(s):  
Vera Trajkovska ◽  
Simka Petrovska-Jovanovic ◽  
Mirko Cvetkovski
Keyword(s):  
Solid Phase Extraction ◽  
Simultaneous Determination ◽  
Water Samples ◽  
Solid Phase ◽  
Detection Limits ◽  
Phase Extraction ◽  
Standard Curve ◽  
Spe Method

Asolid-phase extraction (SPE) method, coupled with HPLC/DAD and GC/FID analysis has been developed for the simultaneous determination of simazine, atrazine and propazine in water samples. The compounds of interest were enriched on Envi-carb SPE tubes. The recoveries for simazine, atrazine and propazine from spiked Nanopure water were 101 5.6 %, 99 4.9 % and 96 5.7 %, respectively. The detection limits were 4.00, 8.00 and 10.00 ng absolute samplemass in the column for simazine, atrazine and propazine, respectively. Standard curve r2 values of 0.9828-0.9988 for the analyzed compounds were consistently obtained.

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