Study on degrees of mesomorphic zone of polymerII. Determination of the degree of mesomorphic zone of eucommia ulmoides gum and natural rubber by dynamic mechanical thermal analysis and differential scanning calorimetry

2017 ◽  
Vol 63 ◽  
pp. 550-557 ◽  
Author(s):  
Jichuan Zhang ◽  
Tianxin Zhang ◽  
Mengjie Dong ◽  
Genshi Liu ◽  
Yiyang Dong
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Natural Rubber ◽  
Dynamic Mechanical Thermal Analysis ◽  
Eucommia Ulmoides ◽  
Scanning Calorimetry ◽  
Dynamic Mechanical ◽  
Eucommia Ulmoides Gum

Miscibiuty in Blends of Polybenzimidazole and Fluorine Containing Polyimides

1989 ◽  
Vol 171 ◽  
Author(s):  
Hiroaki Yamaoka ◽  
Norman E. Aubrey ◽  
William J. MAcknight ◽  
Frank E. Karasz
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Phase Separation ◽  
Dynamic Mechanical Thermal Analysis ◽  
Room Temperature ◽  
Single Phase ◽  
Scanning Calorimetry ◽  
Dynamic Mechanical

ABSTRACTBlends of polybenzimidazole (PBI) with either of two fluorine-containing polyimides were prepared by casting from solution and by precipitation. Dynamic mechanical thermal analysis (DMTA) and differential scanning calorimetry (DSC) were used to study miscibility in the two blend systems.The blends of PBI with the first polyimide, the polysulfonimide Pl-1, consisted of a single phase when the blends contained less than 30 wt% Pl-1; above 50 wt% Pl-1, phase separation occurred even at room temperature. The PBI blends containing the second polyimide, Pl-2, were immiscible.

Determination of Total and Free Water in Triple Superphosphate Fertilizers by Using Thermal Analysis

1985 ◽  
Vol 68 (4) ◽  
pp. 788-793
Author(s):  
Krystyna Kostyrko ◽  
Malgorzata Skoczylas ◽  
Andrzej Klee
Keyword(s):  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Free Water ◽  
Total Water ◽  
Triple Superphosphate ◽  
Scanning Calorimetry ◽  
Thermal Methods ◽  
Dehydration Processes ◽  
Derivatographic Analysis

Abstract Thermal analysis methods were used to study dehydration of triple superphosphate. A redrying procedure followed by Q-derivatographic analysis (under quasiisobaric and quasiisothermal conditions) as well as differential scanning calorimetry (DSC) was applied. Attempts were made to establish the correct drying-oven temperature for determination of water content, i.e., the temperature at which free or total water is removed from the fertilizer. Thermal decomposition of monocalcium orthophosphate monohydrate, the major component of triple superphosphate, was studied and a model was advanced for the reactions that occur during decomposition of this salt. The free water was completely released when superphosphate was heated at a constant temperature of 85°C. The total water was entirely released at 160°C. At 150°C, the process of removing the water of crystallization from the orthophosphate was disturbed by other concomitant dehydration processes which result in irreversible decomposition of this salt. The results obtained indicate that the thermal methods of analysis used are complementary.

The Application of Differential Scanning Calorimetry to Thermal Analysis for Energetic Materials

2013 ◽  
Vol 423-426 ◽  
pp. 588-592
Author(s):  
Yong Kang Chen ◽  
Ming Hua Chen ◽  
Tao Zhang ◽  
Xiao Le Wu
Keyword(s):  
Thermal Stability ◽  
Thermal Analysis ◽  
Differential Scanning Calorimetry ◽  
Thermal Decomposition ◽  
Energetic Materials ◽  
Evaluation Research ◽  
Paper Briefly ◽  
Scanning Calorimetry ◽  
Main Components

Differential Scanning Calorimetry (DSC) is a common and useful method for thermal analysis. This paper briefly introduces the thermal decomposition characteristic determination of the main components of propellant by DSC assay and the applications of DSC in thermal stability and compatibility evaluation research of energetic materials.

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