Two-step heating in the formation of nanosized alumina particles by a pulsed wire discharge method

2011 ◽  
Vol 64 (2) ◽  
pp. 110-113 ◽  
Author(s):  
Satoru Ishihara ◽  
Yuu Shikoda ◽  
Yoshinori Tokoi ◽  
Tadachika Nakayama ◽  
Hisayuki Suematsu ◽  
...  
2016 ◽  
Vol 55 (11) ◽  
pp. 116203
Author(s):  
Jong Hwan Kim ◽  
Dae Sung Kim ◽  
Hisayuki Suematsu ◽  
Bong Ki Ryu

2016 ◽  
Vol 69 (1) ◽  
pp. 36-39 ◽  
Author(s):  
Jong Hwan Kim ◽  
Dae Sung Kim ◽  
Bong Ki Ryu ◽  
Hisayuki Suematsu ◽  
Kenta Tanaka

Author(s):  
Chu Minh Ngo ◽  
Duy Hieu Nguyen ◽  
Thi Mai Dung Do ◽  
Tadachika NAKAYAMA ◽  
Koichi Niihara ◽  
...  

2004 ◽  
Vol 19 (4) ◽  
pp. 1011-1014 ◽  
Author(s):  
H. Suematsu ◽  
K. Ishizaka ◽  
Y. Kinemuchi ◽  
T. Suzuki ◽  
W. Jiang ◽  
...  

Nanosized powders of Ni–Fe–O were synthesized by a pulsed wire discharge method and sintered at 600 °C for 1 h in air. Abrupt electrical resistivity changes were observed in the temperature dependence of resistivity for the sintered Ni–Fe–O powders above 203 °C. Similar resistivity curves, which had been observed in V–O samples and had been used for the critical temperature resistors, had never been reported in Ni–Fe–O samples. Possible mechanisms to explain the resistivity change in NiFe2O4, including order-disorder transition, semiconductor-metal transition, and surface spin pinning, are discussed.


Author(s):  
J. W. Mellowes ◽  
C. M. Chun ◽  
I. A. Aksay

Mullite (3Al2O32SiO2) can be fabricated by transient viscous sintering using composite particles which consist of inner cores of a-alumina and outer coatings of amorphous silica. Powder compacts prepared with these particles are sintered to almost full density at relatively low temperatures (~1300°C) and converted to dense, fine-grained mullite at higher temperatures (>1500°C) by reaction between the alumina core and the silica coating. In order to achieve complete mullitization, optimal conditions for coating alumina particles with amorphous silica must be achieved. Formation of amorphous silica can occur in solution (homogeneous nucleation) or on the surface of alumina (heterogeneous nucleation) depending on the degree of supersaturation of the solvent in which the particles are immersed. Successful coating of silica on alumina occurs when heterogeneous nucleation is promoted and homogeneous nucleation is suppressed. Therefore, one key to successful coating is an understanding of the factors such as pH and concentration that control silica nucleation in aqueous solutions. In the current work, we use TEM to determine the optimal conditions of this processing.


1999 ◽  
Vol 119 (8-9) ◽  
pp. 1084-1089 ◽  
Author(s):  
Haruo Kishida ◽  
Masafumi Tamura ◽  
Yoshiyasu Ehara ◽  
Tairo Ito

Author(s):  
Joseph P. Capesius ◽  
Joseph R. Sullivan ◽  
Gregory B. O'Neill ◽  
Cory A. Williams

Author(s):  
Lotte Melchior Larsen ◽  
David C. Rex ◽  
W. Stuart Watt ◽  
Philip G. Guise

NOTE: This article was published in a former series of GEUS Bulletin. Please use the original series name when citing this article, for example: Melchior Larsen, L., Rex, D. C., Watt, W. S., & Guise, P. G. (1999). 40Ar–39Ar dating of alkali basaltic dykes along the southwest coast of Greenland: Cretaceous and Tertiary igneous activity along the eastern margin of the Labrador Sea. Geology of Greenland Survey Bulletin, 184, 19-29. https://doi.org/10.34194/ggub.v184.5227 _______________ A 380 km long coast-parallel alkali basalt dyke swarm cutting the Precambrian basement in south-western Greenland has generally been regarded as one of the earliest manifestations of rifting during continental stretching prior to break-up in the Labrador Sea. Therefore, the age of this swarm has been used in models for the evolution of the Labrador Sea, although it has been uncertain due to earlier discrepant K–Ar dates. Two dykes from this swarm situated 200 km apart have now been dated by the 40Ar–39Ar step-heating method. Separated biotites yield plateau ages of 133.3 ± 0.7 Ma and 138.6 ± 0.7 Ma, respectively. One of the dykes has excess argon. Plagioclase separates confirm the biotite ages but yield less precise results. The age 133– 138 Ma is earliest Cretaceous, Berriasian to Valanginian, and the dyke swarm is near-coeval with the oldest igneous rocks (the Alexis Formation) on the Labrador shelf. A small swarm of alkali basalt dykes in the Sukkertoppen (Maniitsoq) region of southern West Greenland was also dated. Two separated kaersutites from one sample yield an average plateau age of 55.2 ± 1.2 Ma. This is the Paleocene–Eocene boundary. The swarm represents the only known rocks of that age within several hundred kilometres and may be related to changes in the stress regime during reorganisation of plate movements at 55 Ma when break-up between Greenland and Europe took place.


2016 ◽  
Vol 12 (6) ◽  
pp. 747-753 ◽  
Author(s):  
Marek J. Kasprowicz ◽  
Anna Gorczyca ◽  
Piotr Janas

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