Microwave assisted alkylation of ortho-methyl-tetra-C-naphthyl-resorcinarene and its phosphorylated derivatives with haloalkanes and ethyl bromoacetate

2018 ◽  
Vol 59 (26) ◽  
pp. 2586-2589 ◽  
Author(s):  
Olga S. Serkova ◽  
Valentina V. Glushko ◽  
Maria A. Egorova ◽  
Vera I. Maslennikova
Keyword(s):  
Ethyl Bromoacetate ◽  
Microwave Assisted

Microwave Assisted Synthesis of N-(ethoxycarbonylmethyl)-nucleobases: Building Blocks for PNAs

2005 ◽  
Vol 2005 (3) ◽  
pp. 167-168 ◽  
Author(s):  
Gui-Rong Qu ◽  
Yong Li ◽  
Su-Hui Han
Keyword(s):  
Microwave Irradiation ◽  
Nucleic Acids ◽  
Peptide Nucleic Acids ◽  
Building Blocks ◽  
Microwave Assisted Synthesis ◽  
Ethyl Bromoacetate ◽  
Microwave Assisted

The synthesis of N1/N9- (Ethoxycarbonylmethyl)pyrimidine/purine using as synthons for peptide nucleic acids has been described. Microwave irradiation provided the desired products by alkylation of the appropriately protected natural and substituted nucleobases with ethyl bromoacetate within 4–7 min in 48–85% yields.

Microwave-Assisted Synthesis of Chiral Oxime Ethers

2019 ◽  
Vol 16 (6) ◽  
pp. 495-500
Author(s):  
Asma Mehrez ◽  
Dalila Mtat ◽  
Ridha Touati
Keyword(s):  
Reaction Time ◽  
Microwave Irradiation ◽  
Sodium Hydride ◽  
Second Step ◽  
Chiral Amines ◽  
Microwave Assisted Synthesis ◽  
Ethyl Bromoacetate ◽  
Rapid Synthesis ◽  
New Class ◽  
Microwave Assisted

An efficient and rapid synthesis of a new class of chiral oxime ethers has been achieved via two-step reaction in which the first step is the reaction of oximes 1a-f with ethyl bromoacetate in the presence of sodium hydride to give oxime ethers 2a-f which are subsequently, in the second step, reacted with different commercially available chiral amines under microwave irradiation conditions to give compounds 3a-l in good to excellent yields. Through this method, we have observed a decrease in reaction time and excellent yields than the previously described conventional method.

Microwave-assisted hydrodistillation of essential oil from cherry laurel (Prunus laurocerasus) leaves

Planta Medica ◽  
2009 ◽  
Vol 75 (09) ◽  
Author(s):  
I Stanisavljević ◽  
M Lazić ◽  
N Radulović ◽  
V Veljković
Keyword(s):  
Essential Oil ◽  
Microwave Assisted ◽  
Cherry Laurel ◽  
Prunus Laurocerasus

Microwave-assisted C-H arylation of Quinazolin-4-one-type Precursors of Bioactive Heterocycles

2015 ◽  
Author(s):  
Corinne Fruit ◽  
Julien Godeau ◽  
Marine Harari ◽  
Sylvain Laclef ◽  
Vincent Levacher ◽  
...  
Keyword(s):  
Microwave Assisted ◽  
Bioactive Heterocycles

Microwave-assisted enzymatic hydrolysis of starch

2009 ◽  
Author(s):  
Marcin Lukasiewicz ◽  
Anna Osowiec ◽  
Magdalena Marciniak
Keyword(s):  
Enzymatic Hydrolysis ◽  
Microwave Assisted ◽  
Hydrolysis Of
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