scholarly journals One-step synthesis of black TiO2-x microspheres by ultrasonic spray pyrolysis process and their visible-light-driven photocatalytic activities

2021 ◽  
pp. 105557
Author(s):  
Myeongjun Ji ◽  
Yong-Ho Choa ◽  
Young-In Lee
Metals ◽  
2018 ◽  
Vol 8 (8) ◽  
pp. 569 ◽  
Author(s):  
Elif Emil ◽  
Gözde Alkan ◽  
Sebahattin Gurmen ◽  
Rebeka Rudolf ◽  
Darja Jenko ◽  
...  

Nanostructured zinc oxide (ZnO) particles were synthesized by the one step Ultrasonic Spray Pyrolysis (USP) process from nitrate salt solution (Zn(NO3)2·6H2O). Various influential parameters, from Zn(NO3)2·6H2O concentrations (0.01875–0.0375 M) in the initial solution, carrier gas (N2) flow rates (0.5–0.75 L/min) to reaction temperature (400–800 °C), were tested to investigate their role on the final ZnO particles’ morphology. For this purpose, Scanning Electron Microscopy (SEM), High Resolution Transmission Electron Microscopy (HRTEM) and (Selected Area Electron Diffraction) SAED techniques were used to gain insight into how the ZnO morphology is dependent on the USP process. It was revealed that, by certain parameter selection, different ZnO morphology could be achieved, from spherical to sphere-like structures assembled by interwoven nanoplate and nanoplate ZnO particles. Further, a more detailed crystallographic investigation was performed by XRD and Williamson-Hall (W-H) analysis on the ZnO with unique and non-typical planar morphology that was not reported before by USP synthesis. Moreover, for the first time, a flexible USP formation model was proposed, ending up in various ZnO morphologies rather than only ideal spheres, which is highly promising to target a wide application area.


RSC Advances ◽  
2017 ◽  
Vol 7 (34) ◽  
pp. 21314-21322 ◽  
Author(s):  
Byeong Ho Min ◽  
Kyeong Youl Jung

Spherical carbon spheres with improved mesoporosity and ion sorption properties are synthesized by an ultrasonic spray pyrolysis process from an aqueous sucrose/NaHCO3/TEOS solution.


2005 ◽  
Vol 34 (10) ◽  
pp. 1398-1399 ◽  
Author(s):  
Hung-Chun Wu ◽  
Zheng-Zhao Guo ◽  
Mo-Hua Yang ◽  
Chung-Hsin Lu ◽  
Tai-Yuan Wu ◽  
...  

1998 ◽  
Vol 33 (2) ◽  
pp. 253-260 ◽  
Author(s):  
R Abraham ◽  
F Guenard ◽  
K Lebbou ◽  
S Trosset ◽  
M.T Cohen-Adad ◽  
...  

2016 ◽  
Vol 45 (7) ◽  
pp. 1700-1704 ◽  
Author(s):  
Yin Pengfei ◽  
Sun Lili ◽  
Han Xiangyu ◽  
Xia Chuanhui ◽  
Wu Haiying ◽  
...  

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