A convenient method for synthesis of Fmoc-amino acid p-nitroanilides based on isobutyl chloroformate as condensation agent.

1993 ◽  
Vol 34 (26) ◽  
pp. 4201-4204 ◽  
Author(s):  
Hinyu Nedev ◽  
Hanitra Nabarisoa ◽  
Tomasz Haertle
1977 ◽  
Vol 8 (50) ◽  
pp. no-no
Author(s):  
YU. A. DAVIDOVICH ◽  
V. I. BUTAEVA ◽  
O. M. GALKIN ◽  
T. N. SENTSOVA ◽  
S. V. ROGOZHIN

Some time ago, two of the authors of the present communication, in seeking a method for the separation of the amino-acids from the carbohydrates, found that under certain conditions the former could be readily separated in the form of the barium salts of their carbamates, a class of compounds originally described by Siegfried. As these carbamates, on heating with water, are readily decomposed into barium carbonate and the free amino-acid, it was suggested that a convenient method might be evolved, using the formation of these compounds as a basis, for the separation of the hydrolysis products of the proteins.* This suggestion was followed up, and a method was subsequently elaborated and applied to the separation of the hydrolysis products of gelatin by one of the authors in conjunction with Miss H. L. Kingston. Since the publication of the two papers just quoted, the researches on the use of the “carbamate method,” as it may be conveniently called, have been continued, and promise results, which may ultimately lead to a satisfactory separation of most of the hydrolysis products of the proteins when only relatively small amounts of material are available for investigation. During the course of this work the base, which is the chief subject discussed in this paper, was discovered.


2012 ◽  
Vol 35 (6) ◽  
pp. 1015-1019 ◽  
Author(s):  
Hu Huang ◽  
Wen Jun Xu ◽  
Jing-Yu Jin ◽  
Joon Hee Hong ◽  
Hyun-Jae Shin ◽  
...  

1966 ◽  
Vol 7 (1) ◽  
pp. 33-38 ◽  
Author(s):  
A.A. Kiryushkin ◽  
Yu.A. Ovchinnikov ◽  
M.M. Shemyakin ◽  
V.N. Bochkarev ◽  
B.V. Rozinov ◽  
...  

2021 ◽  
Author(s):  
Andrey Shatskiy ◽  
Anton Axelsson ◽  
Elena Vladimirovna Stepanova ◽  
Jian-Quan Liu ◽  
Temerdashev Azamat ◽  
...  

A protocol for stereoselective C-radical addition to a chiral glyoxylate-derived N-sulfinyl imine was developed through visible light-promoted photoredox catalysis, providing a convenient method for the synthesis of unnatural α-amino acids....


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