Development of Micro-Flame Ionization Detector for Portable Gas Chromatograph

2011 ◽  
Vol 39 (3) ◽  
pp. 439-442 ◽  
Author(s):  
Jian-Wei WANG ◽  
Hong PENG ◽  
Chun-Feng DUAN ◽  
Ya-Feng GUAN
Keyword(s):  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Flame Ionization ◽  
Portable Gas Chromatograph

Micro-flame ionization detector with a novel structure for portable gas chromatograph

Talanta ◽  
2010 ◽  
Vol 82 (3) ◽  
pp. 1022-1026 ◽  
Author(s):  
Jianwei Wang ◽  
Hua Wang ◽  
Chunfeng Duan ◽  
Yafeng Guan
Keyword(s):  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Flame Ionization ◽  
Novel Structure ◽  
Portable Gas Chromatograph

Microdetermination of Ethylene Dibromide in Air by Gas Chromatography

1982 ◽  
Vol 65 (6) ◽  
pp. 1379-1381 ◽  
Author(s):  
T Dumas ◽  
E J Bond
Keyword(s):  
Gas Chromatography ◽  
Ambient Temperature ◽  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Ethylene Dibromide ◽  
Flame Ionization ◽  
Photo Ionization ◽  
Portable Gas Chromatograph ◽  
Aqueous Standard

Abstract Using a new, sensitive photo-ionization detector in a portable gas chromatograph that operates at ambient temperature, a method was developed for determining ethylene dibromide in air as low as 19 ppb. Vapor standards were prepared for calibration of the detector; concentrations in these standards were accurately determined by using a flame ionization detector. This detector was previously calibrated with an aqueous standard of ethylene dibromide. Using the 2 gas chromatographs, the loss of ethylene dibromide through sorption from the atmosphere of the vapor standards was determined. Solubility of ethylene dibromide in water was also established at 3 temperatures, using the flame ionization detector.

Gas-chromatographic method for plasma acetate analysis in acetate-intolerance studies.

1978 ◽  
Vol 24 (2) ◽  
pp. 348-350 ◽  
Author(s):  
L G Nielsen ◽  
K O Ash ◽  
E Thor
Keyword(s):  
Chromatographic Method ◽  
Hemodialysis Patients ◽  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Flame Ionization ◽  
Single Column ◽  
Gas Chromatographic Method

Abstract We describe a modified gas-chromatographic method for acetate in serum or plasma, intended for use in the investigation of acetate intolerance in hemodialysis patients. The assay may be adapted for use with a single-column gas chromatograph equipped with a flame ionization detector. The analysis, made isothermally, requires only 0.5 ml of plasma or serum. Only one deproteinizing step is required to prepare the sample for analysis. Additionally, we present preliminary findings of an ongoing acetate-intolerance study.

GLC Determination of Methanol in Liquids: Collaborative Study

1971 ◽  
Vol 54 (3) ◽  
pp. 558-559
Author(s):  
Donald L Andersen
Keyword(s):  
Collaborative Study ◽  
Flame Ionization Detector ◽  
Specific Method ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Flame Ionization ◽  
Coefficients Of Variation ◽  
Sample Dilution

Abstract A rapid, specific method for methanol in aqueous and nonaqueous liquids has been developed and studied collaboratively. The method involves sample dilution with dioxane to approximately 0.4% methanol and injection into a gas chromatograph fitted with a Porapak R column and a flame ionization detector. A collaborative study, with 7 collaborators each reporting on 6 test portions, showed coefficients of variation of 2.7, 2.1, 2.3, 4.2, 1.8, and 3.5. The method has been adopted as official first action.

scholarly journals Determination of Fatty Acid Composition by a Gas Chromatograph with a Flame Ionization Detector

1973 ◽  
Vol 22 (2) ◽  
pp. 95-101
Author(s):  
Shoichiro WATANABE ◽  
Satoshi NAKASATO ◽  
Hideo KUWAYAMA ◽  
Yukihiro SASAMOTO ◽  
Shinsaku SHIRAISHI ◽  
...  
Keyword(s):  
Fatty Acid Composition ◽  
Fatty Acid ◽  
Acid Composition ◽  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Flame Ionization

Gas-Liquid Chromatographic Determination of Sorbitol in Cooked Sausage Products

1978 ◽  
Vol 61 (1) ◽  
pp. 164-166
Author(s):  
Fred A Moseley ◽  
Joel S Salinsky ◽  
Robert W Woods
Keyword(s):  
Chromatographic Determination ◽  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Simple Method ◽  
Flame Ionization ◽  
Freeze Dried ◽  
Liquid Chromatographic Determination ◽  
Liquid Chromatographic

Abstract A rapid and simple method of analysis has been developed for sorbitol in cooked sausage products. Sorbitol is extracted from cooked sausage products with water, an aliquot of the extract is freeze-dried, and the trimethylsilyl (TMS) derivative of sorbitol is formed. An aliquot of the TMS-sorbitol is injected into a gas chromatograph and measured by a flame ionization detector. Analysis of fortified samples shows that the recovery compares well with known amounts of sorbitol added.

Analyzing volatile organic siloxanes in landfill biogas

2012 ◽  
Vol 39 (6) ◽  
pp. 667-673 ◽  
Author(s):  
Chris Clark ◽  
Richard G. Zytner ◽  
Edward McBean
Keyword(s):  
Best Practices ◽  
Average Concentration ◽  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Analytical Technique ◽  
Flame Ionization ◽  
Volatile Organic ◽  
Reciprocating Engines ◽  
Landfill Biogas

Many municipalities are turning to landfill biogas to generate electricity. A major challenge is the presence of volatile cyclic organic siloxanes in the biogas stream, which upon combustion form silica deposits, decreasing the lifetime and warranty of reciprocating engines and turbines. With literature reporting that the analysis of biogas for siloxanes is complex, an investigation was completed to identify best practices for measuring siloxane concentrations in the biogas. The result is an easy-to-use collection and analytical technique that used commercially available XAD-2 resin ORBO® tubes to capture siloxanes through sorption. Following desorption, analysis was done on a gas chromatograph equipped with a flame ionization detector. Using the developed technique at the Region of Waterloo landfill, the sampled biogas showed the presence of D4-siloxane at an average concentration of 37.6 ± 1.7 mg/m3, while the D5-siloxane concentration was 21.9 ± 1.2 mg/m3. These measured concentrations were higher than those reported by an accredited lab. Investigation suggests that the use of Tedlar® bags by the outside lab to collect the biogas sample affected the reliability and variability of the latter approach.

Gas-Liquid Chromatographic Method for the Analysis of Carbaryl Insecticide Formulations

1974 ◽  
Vol 57 (4) ◽  
pp. 778-780 ◽  
Author(s):  
Lois G Weyer
Keyword(s):  
Chromatographic Method ◽  
Internal Standard ◽  
Direct Analysis ◽  
Flame Ionization Detector ◽  
Gas Chromatograph ◽  
Ionization Detector ◽  
Technical Grade ◽  
Flame Ionization ◽  
Liquid Chromatographic Method ◽  
Liquid Chromatographic

Abstract A gas-liquid chromatographic method has been developed for the direct analysis of Sevin (carbaryl, 1-naphthyl N-methylcarbamate) technical grade, Sevin 85, Sevin 80, and Sevin 50 formulations. The method consists of dissolving the sample in chloroform containing Thiodan as an internal standard; an aliquot of the supernate is injected into a gas chromatograph with a flame ionization detector and a column packed with 3% SE-30 on 60-80 mesh Gas- Chrom Q. The method compares favorably in accuracy with older methods, is not subject to interferences, is rapid, and has automation possibilities.

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