Spatial resolution in electron energy loss scattering

Author(s):  
P.E. Batson ◽  
R.D. Leapman

Limits on the spatial resolution in electron energy loss scattering (EELS) can be classified in several different categories. First, we must consider probe-specimen interactions which are separate from the energy loss event. These produce spreading of the probe in the STEM case and intermixing of beams with different specimen paths in the TEM case. Second, the EELS event itself is dependent on details of the scattering physics. We identify two subcategories for describing this, based roughly on the amount of energy lost -- a) the low energy region including surface and bulk plasmons, and b) core excitations. Third, the statistical quality available for the measurement will degrade the resolution, particularly for core edges.

2013 ◽  
Vol 124 ◽  
pp. 130-138 ◽  
Author(s):  
Jeffery A. Aguiar ◽  
Bryan W. Reed ◽  
Quentin M. Ramasse ◽  
Rolf Erni ◽  
Nigel D. Browning

2016 ◽  
Vol 22 (S3) ◽  
pp. 992-993 ◽  
Author(s):  
Kartik Venkatraman ◽  
Qianlang Liu ◽  
Toshihiro Aoki ◽  
Peter Rez ◽  
Peter A. Crozier

2007 ◽  
Vol 126 (2) ◽  
pp. 024303 ◽  
Author(s):  
M. Hoshino ◽  
K. Sunohara ◽  
C. Makochekanwa ◽  
L. Pichl ◽  
H. Cho ◽  
...  

1993 ◽  
Vol 8 (10) ◽  
pp. 2627-2633 ◽  
Author(s):  
G. Mondio ◽  
F. Neri ◽  
G. Curró ◽  
S. Patané ◽  
G. Compagnini

The dielectric constant of tetracyanoquinodimethane (TCNQ) single crystals has been obtained by reflection electron energy loss spectroscopy (REELS) over the 0–60 eV energy range, using primary electron energies ranging from 0.5 to 1.5 keV at an incidence angle of about 40°. A self-consistent method is discussed concerning the evaluation of the surface and bulk contributions to the loss spectra. As a result, for the first time, the Im(−1/∊) function and the dielectric constant of TCNQ have been deduced in such a wide energy range. According to the results obtained by other authors, the low-energy loss spectral profile is characterized by two main structures ascribed to the π → π∗ dipole-allowed transitions located at about 3.5 and 6.5 eV while, at higher energy loss, the π + σ plasmon, centered at about 21.5 eV, dominates the spectrum. The differences among the spectra taken at different primary energies are interpreted as due only to surface effects, more evident in the low-energy-loss spectral region. The results are in good agreement with those obtained by recent transmission-mode (TEELS) experiments.


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