Multiresidue Method for Determination of 183 Pesticide Residues in Leeks by Rapid Multiplug Filtration Cleanup and Gas Chromatography–Tandem Mass Spectrometry

2015 ◽  
Vol 64 (31) ◽  
pp. 6061-6070 ◽  
Author(s):  
Nan Zou ◽  
Yongtao Han ◽  
Yanjie Li ◽  
Yuhong Qin ◽  
Kejia Gu ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Tandem Mass Spectrometry ◽  
Pesticide Residues ◽  
Tandem Mass ◽  
Multiresidue Method ◽  
Chromatography Tandem Mass Spectrometry

scholarly journals A Rapid and Easy Multiresidue Method for the Determination of Pesticide Residues in Vegetables, Fruits, and Cereals Using Liquid Chromatography/Tandem Mass Spectrometry

2008 ◽  
Vol 91 (4) ◽  
pp. 871-883 ◽  
Author(s):  
Satoshi Takatori ◽  
Masahiro Okihashi ◽  
You Okamoto ◽  
Yoko Kitagawa ◽  
Sachiko Kakimoto ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Liquid Chromatography ◽  
Tandem Mass Spectrometry ◽  
Pesticide Residues ◽  
Agricultural Products ◽  
Tandem Mass ◽  
Multiresidue Method ◽  
Chromatography Tandem Mass Spectrometry ◽  
Liquid Chromatography Tandem Mass

Abstract The applicability of a rapid and easy multiresidue method for determination of pesticide residues in agricultural products by using liquid chromatography/tandem mass spectrometry (LC/MS/MS) was examined. Pesticide residues were extracted with acetonitrile in a disposable tube using a homogenizer, followed by salting out with anhydrous magnesium sulfate and sodium chloride. The extract was purified with a double-layered cartridge column (graphite carbon black/primary-secondary amine silica gel). After removal of the solvent, the extract was resolved in methanolwater and analyzed with LC/MS/MS. Recovery tests of 99 pesticide residues from 7 agricultural products were performed at 20 and 100 ng/g. Throughout all of the agricultural products tested, 47 pesticides exhibited satisfactory recoveries (70120) and relative standard deviations (<20) at both concentrations. The time for processing of 12 samples to test solutions was approximately 23 h. This method could be useful for determination of pesticide residues in agricultural products.

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