Controlling Zeolitic Imidazolate Framework Nano- and Microcrystal Formation: Insight into Crystal Growth by Time-Resolved In Situ Static Light Scattering

2011 ◽  
Vol 23 (8) ◽  
pp. 2130-2141 ◽  
Author(s):  
Janosch Cravillon ◽  
Roman Nayuk ◽  
Sergej Springer ◽  
Armin Feldhoff ◽  
Klaus Huber ◽  
...  
2016 ◽  
Vol 16 (4) ◽  
pp. 2002-2010 ◽  
Author(s):  
Sanjib Saha ◽  
Sergej Springer ◽  
Maria E. Schweinefuß ◽  
Diego Pontoni ◽  
Michael Wiebcke ◽  
...  

2021 ◽  
Author(s):  
Matthias Schwartzkopf ◽  
Sven-Jannik Wöhnert ◽  
Vivian Waclawek ◽  
Niko Carstens ◽  
André Rothkirch ◽  
...  

At the nascence of a metal–polymer hybrid material primarily vertical Au dimers and free adatoms diffuse on and into the polymer matrix revealed in situ by sub-millisecond time-resolved surface-sensitive X-ray scattering (GISAXS).


2013 ◽  
Vol 117 (48) ◽  
pp. 15165-15175 ◽  
Author(s):  
Rolf Michels ◽  
Yvonne Hertle ◽  
Thomas Hellweg ◽  
Klaus Huber

1980 ◽  
Vol 1 ◽  
Author(s):  
G.L. Olson ◽  
S.A. Kokorowski ◽  
J.A. Roth ◽  
L.D. Hess

ABSTRACTWe report the use of time-resolved optical reflectivity to directly monitor the dynamics of cw laser-induced solid phase epitaxy (SPE) of thin films. This in situ measurement technique utilizes optical interference effects between light reflected from the surface of a sample and from an advancing interface to provide continuous temporal and spatial resolution of crystal growth processes. SPE growth rates of ionimplanted films which are five orders of magnitude faster than previously observed can be induced and accurately measured with the laser method. Arsenic enhances the SPE rate, and spatially resolved measurements show that the growth rate for arsenic implanted films varies in accordance with the ionimplantation profile. Results are reported for silicon selfimplanted samples with and without subsequent arsenic ion implantation, and for silicon samples directly implanted with arsenic.


2014 ◽  
Vol 70 (a1) ◽  
pp. C855-C855
Author(s):  
Karena Chapman

In the last decade, the potential of the pair distribution function (PDF) method as a versatile tool for materials characterization has expanded enormously, driven by accelerated data acquisition (from hours to sub-second) and the advent of dedicated PDF instruments, such as 11-ID-B at the Advanced Photon Source. New time-resolved, in-situ/operando, parametric, and combined experimental capabilities coupled with innovative model-independent approaches to data analysis are being developed to harness the growing potential of this methodology. For example, while the complex multicomponent architecture of batteries and their coupled electronic, chemical and structural transformations complicate investigations of functionality, through the development of new insitu PDF measurement capabilities and analytical approaches, we have been able to gain insight into the structure and reactivity of these electrochemical energy storage systems.[1] This presentation will describe recent studies of electrode reactions during cycling and the atomic structure of electrolytes.[2]


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