Exchange of axial and equatorial carbonyl groups in pentacoordinate metal carbonyls in the solid state. The variable temperature magic angle spinning carbon-13 NMR spectroscopy of iron pentacarbonyl, [Ph3PNPPh3][HFe(CO)4], and [NEt4][HFe(CO)4]

1990 ◽  
Vol 112 (3) ◽  
pp. 974-977 ◽  
Author(s):  
Brian E. Hanson ◽  
Kenton H. Whitmire
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Variable Temperature ◽  
Iron Pentacarbonyl ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Carbonyl Groups ◽  
Metal Carbonyls ◽  
Angle Spinning

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

51V Solid-State Magic Angle Spinning NMR Spectroscopy and DFT Studies of Oxovanadium(V) Complexes Mimicking the Active Site of Vanadium Haloperoxidases

2003 ◽  
Vol 42 (4) ◽  
pp. 1256-1266 ◽  
Author(s):  
Neela Pooransingh ◽  
Ekaterina Pomerantseva ◽  
Martin Ebel ◽  
Sven Jantzen ◽  
Dieter Rehder ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Active Site ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Dft Studies ◽  
Angle Spinning

SOLARIA: A Protocol for Automated Cross-Peak Assignment and Structure Calculation for Solid-State Magic-Angle Spinning NMR Spectroscopy

2005 ◽  
Vol 117 (38) ◽  
pp. 6307-6310 ◽  
Author(s):  
Michele Fossi ◽  
Federica Castellani ◽  
Michael Nilges ◽  
Hartmut Oschkinat ◽  
Barth-Jan van Rossum
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Magic Angle Spinning ◽  
Structure Calculation ◽  
Cross Peak ◽  
Magic Angle ◽  
Peak Assignment ◽  
Angle Spinning
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