A New Approach in 1D and 2D13C High-Resolution Solid-State NMR Spectroscopy of Paramagnetic Organometallic Complexes by Very Fast Magic-Angle Spinning

2003 ◽  
Vol 125 (12) ◽  
pp. 3438-3439 ◽  
Author(s):  
Yoshitaka Ishii ◽  
Nalinda P. Wickramasinghe ◽  
Sandra Chimon
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Organometallic Complexes ◽  
Magic Angle ◽  
New Approach ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

Band-Selective1H−13C Cross-Polarization in Fast Magic Angle Spinning Solid-State NMR Spectroscopy

2008 ◽  
Vol 130 (51) ◽  
pp. 17216-17217 ◽  
Author(s):  
Ségolène Laage ◽  
Alessandro Marchetti ◽  
Julien Sein ◽  
Roberta Pierattelli ◽  
Hans Juergen Sass ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Cross Polarization ◽  
Solid State Nmr Spectroscopy ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning
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