scholarly journals Chemical Composition of Vintage Preban Absinthe with Special Reference to Thujone, Fenchone, Pinocamphone, Methanol, Copper, and Antimony Concentrations

2008 ◽  
Vol 56 (9) ◽  
pp. 3073-3081 ◽  
Author(s):  
Dirk W. Lachenmeier ◽  
David Nathan-Maister ◽  
Theodore A. Breaux ◽  
Eva-Maria Sohnius ◽  
Kerstin Schoeberl ◽  
...  
Author(s):  
M. V. Lagoyskaya

Сonsiders the possibility of analyzing samples of small diameters without the use of special adapters for determining the chemical composition on spectrometers. Measurements are limited to the size of the hole on the analytical table, which is 12 mm. Accordingly, all analyzed samples must have a diameter of at least 14 mm to completely cover the sample cover of the discharge chamber in order to avoid air entering the chamber. The company manufacturer of spectral equipment offers to use special adapters for the analysis of small samples. But the use of such adapters has a number of drawbacks. These include additional cash costs for the purchase of adapters, the need for additional standardization procedures, the availability of special reference samples. In the laboratory of analytical support (LAS) of the Central Laboratory of the Factory (CLF), all samples of finished rolled products (wire rods or fittings) in size from 5.5 mm to 20 mm are prepared in the form of «blades». The compressed part of the «blade» is the analyzed surface of the sample, which is further processed on a disk grinder and transmitted to the spectral analysis. The article presents the results of comparative tests of valves class U500 between samples in the form of «blades» and in the form of «columns» and concluded that the necessity of use of special adapters.


1966 ◽  
Vol 6 (22) ◽  
pp. 266 ◽  
Author(s):  
CT Gates ◽  
JR Wilson ◽  
NH Shaw

The chemical composition of Stylosanthes humilis H.B.K. in response to a factorial combination of phosphorus, sulphur, molybdenum, and calcium carbonate treatments was studied with special reference to cation composition and protein synthesis. The aim was to assess the potential of S. humilis to adapt to a wide range of nutrient treatments. Protein synthesis was enhanced by high phosphorus-high sulphur treatments, and was accompanied by a low soluble : residual nitrogen ratio. This occurred despite the development of an apparent potassium shortage at this treatment combination. High phosphorus-high sulphur plants had low potassium : sodium ratios, and, although large, their potassium content was below critical levels (9-14 m.-equiv. per 100g). Potassium was partially substituted for by sodium and to a lesser degree by magnesium under these conditions. Although high protein levels were achieved, the full potential for protein synthesis did not seem to be attained by reason of the potassium shortage which developed. S. humilis was able to grow and fix significant quantities of nitrogen that bore a close relation at all levels to the wide range in chemical composition and yield response that developed with treatment.


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