Mechanism of Solid-State Thermolysis of Ammonia Borane: A 15N NMR Study Using Fast Magic-Angle Spinning and Dynamic Nuclear Polarization

2014 ◽  
Vol 118 (34) ◽  
pp. 19548-19555 ◽  
Author(s):  
Takeshi Kobayashi ◽  
Shalabh Gupta ◽  
Marc A. Caporini ◽  
Vitalij K. Pecharsky ◽  
Marek Pruski
Keyword(s):  
Solid State ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Ammonia Borane ◽  
Magic Angle Spinning ◽  
15N Nmr ◽  
Magic Angle ◽  
Nmr Study ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

scholarly journals 19F Dynamic Nuclear Polarization at Fast Magic Angle Spinning for NMR of HIV-1 Capsid Protein Assemblies

2019 ◽  
Vol 141 (14) ◽  
pp. 5681-5691 ◽  
Author(s):  
Manman Lu ◽  
Mingzhang Wang ◽  
Ivan V. Sergeyev ◽  
Caitlin M. Quinn ◽  
Jochem Struppe ◽  
...  
Keyword(s):  
Capsid Protein ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Protein Assemblies ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning ◽  
Hiv 1

scholarly journals Dynamic Nuclear Polarization Efficiency Increased by Very Fast Magic Angle Spinning

2017 ◽  
Vol 139 (31) ◽  
pp. 10609-10612 ◽  
Author(s):  
Sachin R. Chaudhari ◽  
Dorothea Wisser ◽  
Arthur C. Pinon ◽  
Pierrick Berruyer ◽  
David Gajan ◽  
...  
Keyword(s):  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

Dynamic Nuclear Polarization-Enhanced Biomolecular NMR Spectroscopy at High Magnetic Field with Fast Magic-Angle Spinning

2018 ◽  
Vol 130 (25) ◽  
pp. 7580-7584 ◽  
Author(s):  
Kristaps Jaudzems ◽  
Andrea Bertarello ◽  
Sachin R. Chaudhari ◽  
Andrea Pica ◽  
Diane Cala-De Paepe ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Nmr Spectroscopy ◽  
High Magnetic Field ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Biomolecular Nmr ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

scholarly journals Photo-CIDNP in Solid State

2021 ◽  
Author(s):  
Jörg Matysik ◽  
Yonghong Ding ◽  
Yunmi Kim ◽  
Patrick Kurle ◽  
Alexandra Yurkovskaya ◽  
...  
Keyword(s):  
Solid State ◽  
Dynamic Nuclear Polarization ◽  
Analytical Method ◽  
Nuclear Polarization ◽  
State Of The Art ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Radical Pairs ◽  
Chemically Induced ◽  
Angle Spinning

AbstractPhoto-CIDNP (photo-chemically induced dynamic nuclear polarization) refers to nuclear polarization created by the spin-chemical evolution of spin-correlated radical pairs (SCRPs). This phenomenon occurs in gases, liquids and solids. Based on the solid-state photo-CIDNP effect observed under magic-angle spinning (MAS), photo-CIDNP MAS NMR has been developed as analytical method. Here we report the origin, the theory and the state of the art of this method.

scholarly journals Optimizing nitroxide biradicals for cross-effect MAS-DNP: the role of g-tensors’ distance

2020 ◽  
Vol 22 (6) ◽  
pp. 3643-3652 ◽  
Author(s):  
Frédéric Mentink-Vigier
Keyword(s):  
Solid State ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Cross Effect ◽  
Angle Spinning

Nitroxide biradicals are common polarizing agents used to enhance the sensitivity of solid-state NMR experiments via Magic Angle Spinning Dynamic Nuclear Polarization (MAS-DNP).

scholarly journals Natural Abundance Oxygen-17 Solid-State NMR of Metal Organic Frameworks Enhanced by Dynamic Nuclear Polarization

2021 ◽  
Author(s):  
Diego Carnevale ◽  
Georges Mouchaham ◽  
Sujing WANG ◽  
Mathieu Baudin ◽  
Christian SERRE ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Dynamic Nuclear Polarization ◽  
Solid State Nmr ◽  
Nuclear Polarization ◽  
Metal Organic Frameworks ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Metal Organic ◽  
Angle Spinning

The 17O resonances of Zirconium-oxo clusters in porous Zr carboxylate metal-organic frameworks (MOFs) have been investigated by magic-angle spinning (MAS) NMR spectroscopy enhanced by dynamic nuclear polarization (DNP) at natural...

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