Backbone assignment of perdeuterated proteins by solid-state NMR using proton detection and ultrafast magic-angle spinning

2017 ◽  
Vol 12 (4) ◽  
pp. 764-782 ◽  
Author(s):  
Pascal Fricke ◽  
Veniamin Chevelkov ◽  
Maximilian Zinke ◽  
Karin Giller ◽  
Stefan Becker ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Backbone Assignment ◽  
Magic Angle ◽  
Proton Detection ◽  
Perdeuterated Proteins ◽  
Angle Spinning

Enhanced Resolution and Coherence Lifetimes in the Solid-State NMR Spectroscopy of Perdeuterated Proteins under Ultrafast Magic-Angle Spinning

2011 ◽  
Vol 2 (17) ◽  
pp. 2205-2211 ◽  
Author(s):  
Józef R. Lewandowski ◽  
Jean-Nicolas Dumez ◽  
Ümit Akbey ◽  
Sascha Lange ◽  
Lyndon Emsley ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Solid State Nmr Spectroscopy ◽  
Perdeuterated Proteins ◽  
Enhanced Resolution ◽  
Angle Spinning

scholarly journals Rapid access to RNA resonances by proton-detected solid-state NMR at >100 kHz MAS

2018 ◽  
Vol 54 (65) ◽  
pp. 8972-8975 ◽  
Author(s):  
Alexander Marchanka ◽  
Jan Stanek ◽  
Guido Pintacuda ◽  
Teresa Carlomagno
Keyword(s):  
Molecular Weight ◽  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Spin Systems ◽  
Magic Angle ◽  
Proton Detection ◽  
Rapid Access ◽  
Highly Sensitive ◽  
Angle Spinning

Fast (>100 kHz) magic angle spinning solid-state NMR allows combining high-sensitive proton detection with the absence of an intrinsic molecular weight limit. Here we apply this technique to RNA and assign nucleotide spin systems through highly sensitive multidimensional experiments.

scholarly journals Enhancing the Sensitivity of Solid-State NMR Experiments with Very Low Gyromagnetic Ratio Nuclei with Fast Magic Angle Spinning and Proton Detection

2018 ◽  
Vol 122 (25) ◽  
pp. 5635-5643 ◽  
Author(s):  
Amrit Venkatesh ◽  
Matthew J. Ryan ◽  
Abhranil Biswas ◽  
Kasuni C. Boteju ◽  
Aaron D. Sadow ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Gyromagnetic Ratio ◽  
Magic Angle ◽  
Proton Detection ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

scholarly journals Combination of solid state NMR and DFT calculation to elucidate the state of sodium in hard carbon electrodes

2016 ◽  
Vol 4 (34) ◽  
pp. 13183-13193 ◽  
Author(s):  
Ryohei Morita ◽  
Kazuma Gotoh ◽  
Mika Fukunishi ◽  
Kei Kubota ◽  
Shinichi Komaba ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Dft Calculation ◽  
Magic Angle Spinning ◽  
The State ◽  
Mas Nmr ◽  
Magic Angle ◽  
Multiple Quantum ◽  
Hard Carbon ◽  
Angle Spinning

We examined the state of sodium electrochemically inserted in HC prepared at 700–2000 °C using solid state Na magic angle spinning (MAS) NMR and multiple quantum (MQ) MAS NMR.

Rotational resonance for a heteronuclear spin pair under magic-angle spinning in solid-state NMR

2017 ◽  
Vol 146 (15) ◽  
pp. 154202
Author(s):  
Takayuki Kamihara ◽  
K. Takegoshi
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Rotational Resonance ◽  
Spin Pair ◽  
Angle Spinning
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