scholarly journals Rapid access to RNA resonances by proton-detected solid-state NMR at >100 kHz MAS

2018 ◽  
Vol 54 (65) ◽  
pp. 8972-8975 ◽  
Author(s):  
Alexander Marchanka ◽  
Jan Stanek ◽  
Guido Pintacuda ◽  
Teresa Carlomagno
Keyword(s):  
Molecular Weight ◽  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Spin Systems ◽  
Magic Angle ◽  
Proton Detection ◽  
Rapid Access ◽  
Highly Sensitive ◽  
Angle Spinning

Fast (>100 kHz) magic angle spinning solid-state NMR allows combining high-sensitive proton detection with the absence of an intrinsic molecular weight limit. Here we apply this technique to RNA and assign nucleotide spin systems through highly sensitive multidimensional experiments.

Backbone assignment of perdeuterated proteins by solid-state NMR using proton detection and ultrafast magic-angle spinning

2017 ◽  
Vol 12 (4) ◽  
pp. 764-782 ◽  
Author(s):  
Pascal Fricke ◽  
Veniamin Chevelkov ◽  
Maximilian Zinke ◽  
Karin Giller ◽  
Stefan Becker ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Backbone Assignment ◽  
Magic Angle ◽  
Proton Detection ◽  
Perdeuterated Proteins ◽  
Angle Spinning

scholarly journals Combination of solid state NMR and DFT calculation to elucidate the state of sodium in hard carbon electrodes

2016 ◽  
Vol 4 (34) ◽  
pp. 13183-13193 ◽  
Author(s):  
Ryohei Morita ◽  
Kazuma Gotoh ◽  
Mika Fukunishi ◽  
Kei Kubota ◽  
Shinichi Komaba ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Dft Calculation ◽  
Magic Angle Spinning ◽  
The State ◽  
Mas Nmr ◽  
Magic Angle ◽  
Multiple Quantum ◽  
Hard Carbon ◽  
Angle Spinning

We examined the state of sodium electrochemically inserted in HC prepared at 700–2000 °C using solid state Na magic angle spinning (MAS) NMR and multiple quantum (MQ) MAS NMR.

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

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