Nitrophenyl derivatives of pyrrole 2,5-diamides: structural behaviour, anion binding and colour change signalled deprotonationElectronic supplementary information (ESI) available: 1H NMR, 13C NMR and mass spectra for compounds 2 and 3, NMR anion titration profiles in DMSO-d6–0.5% water. See http://www.rsc.org/suppdata/ob/b2/b210848h/

Salvatore Camiolo; Philip A. Gale; Michael B. Hursthouse; Mark E. Light

doi:10.1039/b210848h

Nitrophenyl derivatives of pyrrole 2,5-diamides: structural behaviour, anion binding and colour change signalled deprotonationElectronic supplementary information (ESI) available: 1H NMR, 13C NMR and mass spectra for compounds 2 and 3, NMR anion titration profiles in DMSO-d6–0.5% water. See http://www.rsc.org/suppdata/ob/b2/b210848h/

Organic & Biomolecular Chemistry ◽

10.1039/b210848h ◽

2003 ◽

Vol 1 (4) ◽

pp. 741-744 ◽

Cited By ~ 160

Author(s):

Salvatore Camiolo ◽

Philip A. Gale ◽

Michael B. Hursthouse ◽

Mark E. Light

Keyword(s):

1H Nmr ◽

13C Nmr ◽

Mass Spectra ◽

Colour Change ◽

Anion Binding ◽

Supplementary Information ◽

Structural Behaviour ◽

Derivatives Of

Synthesis and Anticonvulsant Activity of 3-(alkylamino, alkoxy)-1,3,4,5- Tetrahydro-2H-benzo [b] azepine-2-one Derivatives

CNS & Neurological Disorders - Drug Targets ◽

10.2174/1871527317666180704101332 ◽

2018 ◽

Vol 17 (6) ◽

pp. 448-457 ◽

Cited By ~ 1

Author(s):

Xia Huang ◽

Tie Chen ◽

Rong-Bi Han ◽

Feng-Yu Piao

Keyword(s):

1H Nmr ◽

Elemental Analysis ◽

13C Nmr ◽

Anticonvulsant Activity ◽

Mass Spectra ◽

Maximal Electroshock ◽

Test Compound ◽

Maximal Electroshock Test ◽

Mes Test ◽

Structure Activity

Background & Objective: A series of novel 3-Substituted-1,3,4,5-Tetrahydro-2H-benzo [b] azepine-2-one Derivatives (4, 5, 7, 10, 12, 5a-j, 8a-e) were synthesized from 1,2,3,4-Tetrahydro-1- naphthalenone. The structures of these compounds were confirmed by IR, 1H NMR, 13C NMR, MASS spectra and elemental analysis. Their anticonvulsant activity was evaluated by the maximal electroshock (MES) test, subcutaneous pentylenetetrazol (scPTZ) test, and their neurotoxicity was evaluated by the rotarod neurotoxicity test. Compound 4 showed the maximum anticonvulsant activity against the maximal electroshock test (ED50=26.4, PI =3.2) and against the subcutaneous pentylenetetrazol test (ED50=40.2, PI =2.1). Conclusion: Possible structure-activity relationship was discussed.

Tandem RCM-Pauson–Khand reaction for access to tricycles in one stepElectronic supplementary information (ESI) available: spectral data and 1H-NMR and 13C-NMR spectra for compounds 8, 10, 11, 14a and 14b. See http://www.rsc.org/suppdata/ob/b3/b302277c

Organic & Biomolecular Chemistry ◽

10.1039/b302277c ◽

2003 ◽

Vol 1 (9) ◽

pp. 1450-1451 ◽

Cited By ~ 21

Author(s):

Marta Rosillo ◽

Luis Casarrubios ◽

Gema Domínguez ◽

Javier Pérez-Castells

Keyword(s):

Spectral Data ◽

1H Nmr ◽

13C Nmr ◽

Nmr Spectra ◽

Supplementary Information ◽

13C Nmr Spectra

1H NMR, 13C NMR and mass spectra of some chlorocymenes

Chemosphere ◽

10.1016/0045-6535(89)90082-9 ◽

1989 ◽

Vol 19 (8-9) ◽

pp. 1349-1356 ◽

Cited By ~ 3

Author(s):

Tauno Kuokkanen

Keyword(s):

1H Nmr ◽

13C Nmr ◽

Mass Spectra

A novel crownophane trapping CO2 as carbonic acid at room temperatureElectronic supplementary information (ESI) available: synthesis of compounds, 2 ? 4, and the data of their 1H NMR, IR, ESI mass spectra and elemental analysis, and the charts of IR spectrum and DTA and TGA thermograms of the solids separated out after bubbling CO2. See http://www.rsc.org/suppdata/cc/b4/b403152k/

Chemical Communications ◽

10.1039/b403152k ◽

2004 ◽

pp. 1474 ◽

Cited By ~ 11

Author(s):

Kazuhisa Hiratani ◽

Nobuko Sakamoto ◽

Naohiro Kameta ◽

Michinori Karikomi ◽

Yoshinobu Nagawa

Keyword(s):

1H Nmr ◽

Elemental Analysis ◽

Ir Spectrum ◽

Mass Spectra ◽

Carbonic Acid ◽

Supplementary Information

Isolation and characterization of iridium(iii) and iridium(v) complexes of 2-(arylazo)pyridine and studies of amine fusion reactions at the coordinated diazo-ligandElectronic supplementary information (ESI) available: Fig. S1: 1H NMR spectra of 1a and tcc-[RuCl2(HL1a)2] in CDCl3. Inset: Methyl resonances of 1b. Fig. S2: 13C NMR spectra of 1a and tcc-[RuCl2(HL1a)2] in CDCl3. Fig. S3: Cyclic voltammogram of 1a in CH3CN. Fig. S4: Cyclic voltammogram of 2a in CH3CN. See http://www.rsc.org/suppdata/dt/b4/b407209j/

Dalton Transactions ◽

10.1039/b407209j ◽

2004 ◽

pp. 2655 ◽

Cited By ~ 20

Author(s):

Manashi Panda ◽

Chayan Das ◽

Gene-Hsiang Lee ◽

Shie-Ming Peng ◽

Sreebrata Goswami

Keyword(s):

1H Nmr ◽

13C Nmr ◽

Nmr Spectra ◽

1H Nmr Spectra ◽

Supplementary Information ◽

Cyclic Voltammogram ◽

13C Nmr Spectra ◽

Fusion Reactions ◽

Isolation And Characterization

Spontaneous disproportionation of rhodium(i) bisoxazolinates to rhodium(ii)Electronic supplementary information (ESI) available: synthetic procedures (including 1H NMR, 13C NMR and elemental analysis data), EPR spectrum and cyclic voltammogram. See http://www.rsc.org/suppdata/cc/b1/b110183h/

Chemical Communications ◽

10.1039/b110183h ◽

2002 ◽

pp. 148-149 ◽

Cited By ~ 10

Author(s):

Sander T. H. Willems ◽

Jaap C. Russcher ◽

Peter H. M. Budzelaar ◽

Bas de Bruin ◽

René de Gelder ◽

...

Keyword(s):

1H Nmr ◽

Elemental Analysis ◽

13C Nmr ◽

Analysis Data ◽

Supplementary Information ◽

Elemental Analysis Data ◽

Cyclic Voltammogram ◽

Epr Spectrum ◽

Electronic Supplementary Information

EXTRACTION, ISOLATION AND SYNTHESIS OF DERIVATIVES OF URSOLIC ACID

INDIAN DRUGS ◽

10.53879/id.49.01.p0033 ◽

2012 ◽

Vol 49 (01) ◽

pp. 33-37

Author(s):

S. B. Babar ◽

◽

K. S. Laddha

Keyword(s):

Petroleum Ether ◽

Ursolic Acid ◽

1H Nmr ◽

13C Nmr ◽

Methanol Extract ◽

Nmr Studies ◽

Simple Method ◽

Synthetic Derivatives ◽

Derivatives Of

Study was undertaken with an objective to develop a simple method for isolation of ursolic acid from Nerium indicum Mill leaves and to prepare synthetic derivatives of ursolic acid. The leaves were defatted with petroleum ether and then extracted with methanol. Methanol extract was basified and subsequently acidified, followed by charcoal treatment to isolate ursolic acid. Synthetic derivatives were prepared from isolated ursolic acid by substitution at C-3 position. The structure of ursolic acid and its derivatives were confirmed by IR, MS, 1H NMR, 13C NMR studies.

Development of a temporary marker for peptidesElectronic supplementary information (ESI) available: IR, UV, 1H NMR and 13C NMR spectra of compounds 2a–i, 3b–h, 4b–h, 5, 6c and h, 7h, 8–12, 13c and h, and 14. See http://www.rsc.org/suppdata/ob/b2/b212470j/

Organic & Biomolecular Chemistry ◽

10.1039/b212470j ◽

2003 ◽

Vol 1 (9) ◽

pp. 1480-1485 ◽

Cited By ~ 5

Author(s):

M. Sameiro T. Gonçalves ◽

Hernâni L. S. Maia

Keyword(s):

1H Nmr ◽

13C Nmr ◽

Nmr Spectra ◽

Supplementary Information ◽

13C Nmr Spectra

ZrCl4-promoted halogen migration during an electrophilic amination of halogenated phenolsElectronic supplementary information (ESI) available: spectroscopic data (1H NMR,13C NMR, IR, MS), mp and elemental analysis (or HRMS) for the products 3 and 4. See http://www.rsc.org/suppdata/cc/b2/b203622c/Dedicated to Professor Waldemar Adam, University of Würzburg, Germany, on the occasion of his 65th birthday.

Chemical Communications ◽

10.1039/b203622c ◽

2002 ◽

pp. 1494-1495 ◽

Cited By ~ 22

Author(s):

Sergeja Bombek ◽

Roman Lenaršič ◽

Marijan Kočevar ◽

Laurent Saint-Jalmes ◽

Jean-Roger Desmurs ◽

...

Keyword(s):

1H Nmr ◽

Elemental Analysis ◽

13C Nmr ◽

Spectroscopic Data ◽

Supplementary Information ◽

65Th Birthday ◽

Electrophilic Amination

Photo-induced energy transfer and its switching in dyad and triad chromophore systems composed of coumarin, Ru(ii) and Os(ii) terpyridine-type complexesElectronic supplementary information (ESI) available: 1H NMR and ES mass spectra of the new dyad and triad coumarin-containing complexes, (C151)2-Os, (C151)2-Ru-ph-Os and (C151)2-Ru-azo-Os and the emission spectra of (C151)2-tpy and (C151)2-Os. See http://www.rsc.org/suppdata/dt/b2/b212274j/

Dalton Transactions ◽

10.1039/b212274j ◽

2003 ◽

pp. 1537-1544 ◽

Cited By ~ 32

Author(s):

Tetsuo Akasaka ◽

Toshiki Mutai ◽

Joe Otsuki ◽

Koji Araki

Keyword(s):

Energy Transfer ◽

1H Nmr ◽

Mass Spectra ◽

Emission Spectra ◽

Supplementary Information