Synthesis and crystal structure of a nonionic compound of sodium, (1-phenylbutane-1,3-dionato)(ethylene glycol)sodium

1970 ◽  
pp. 49 ◽  
Author(s):  
D. Bright ◽  
A. J. Kolombos ◽  
G. H. W. Milburn ◽  
R. S. Nyholm ◽  
Mary R. Truter
Keyword(s):  
Crystal Structure ◽  
Ethylene Glycol ◽  
Synthesis And Crystal Structure

scholarly journals Synthesis and crystal structure of triethylammonium hexabromidouranate(IV) dichloromethane monosolvate

2020 ◽  
Vol 76 (10) ◽  
pp. 1587-1590
Author(s):  
Holger Lars Deubner ◽  
Marcel Koester ◽  
Carsten von Haenisch ◽  
Florian Kraus
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bond ◽  
Low Temperature ◽  
Ethylene Glycol ◽  
Network Structure ◽  
Three Dimensional ◽  
Uranium Atom ◽  
Synthesis And Crystal Structure ◽  
Dimensional Network ◽  
Solvent Molecules

Triethylammonium hexabromidouranate(IV) dichloromethane monosolvate, [(C2H5)3NH]2[UBr6]·CH2Cl2, was obtained in the form of dark-brown crystals from the reaction of uranium pentabromide with NEt3 and ethylene glycol in dichloromethane at low temperature. During the progress of the reaction, the reduction of uranium(V) to uranium(IV) was observed, whose associated oxidation product could not be identified. The uranium atom of the [UBr6]2– anion is coordinated by six bromido ligands in the shape of an octahedron. Between cations, anion and solvent molecules of crystallization, numerous C—H...Hal hydrogen-bond-like interactions are present, leading to a three-dimensional network structure.

Synthesis and crystal structure of [MnL(μ-Cl)MnCl3]·H2O L=N, N'-bis(2'-pyridine)methyl-1,10-phenanthroline-2,9-dimethanamine

2002 ◽  
Vol 2002 (3) ◽  
pp. 120-121
Author(s):  
Tian Fu Liu ◽  
Hua Kuan Lin ◽  
Shou Rong Zhu ◽  
Zhong Ming Wang ◽  
Hong Gen Wang ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure

Synthesis and crystal structure of an 18-Mo girdle-like polyoxomolybdate

2002 ◽  
Vol 2002 (3) ◽  
pp. 107-109 ◽  
Author(s):  
Guang Liu ◽  
Jian Liu ◽  
Shi-Wei Zhang
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure

The Synthesis and Crystal Structure of Aluminum Selenite Trihydrate, Al2(seO3)3.32O

1992 ◽  
Author(s):  
W. T. Harrison ◽  
G. D. Stucky ◽  
R. E. Morris ◽  
A. K. Cheetham
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure

scholarly journals High-pressure synthesis and crystal structure of the mixed-cation borate Ga4In4B15O33(OH)3

2019 ◽  
Vol 74 (4) ◽  
pp. 357-363
Author(s):  
Daniela Vitzthum ◽  
Hubert Huppertz
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Diffraction Data ◽  
X Ray Diffraction ◽  
Synthesis And Crystal Structure ◽  
X Ray ◽  
Mixed Cation ◽  
High Pressure High Temperature ◽  
Pressure Synthesis

AbstractThe mixed cation triel borate Ga4In4B15O33(OH)3 was synthesized in a Walker-type multianvil apparatus at high-pressure/high-temperature conditions of 12.5 GPa and 1300°C. Although the product could not be reproduced in further experiments, its crystal structure could be reliably determined via single-crystal X-ray diffraction data. Ga4In4B15O33(OH)3 crystallizes in the tetragonal space group I41/a (origin choice 2) with the lattice parameters a = 11.382(2), c = 15.244(2) Å, and V = 1974.9(4) Å3. The structure of the quaternary triel borate consists of a complex network of BO4 tetrahedra, edge-sharing InO6 octahedra in dinuclear units, and very dense edge-sharing GaO6 octahedra in tetranuclear units.

scholarly journals Synthesis and Crystal Structure of the Bis(μ-hydroxo)diiron(II) Complex with Tridentate Ligands Having a Sterically Bulky Imidazolyl Group

2019 ◽  
Vol 35 (0) ◽  
pp. 27-29
Author(s):  
Reiko YAGUCHI ◽  
Hideki FURUTACHI ◽  
Sanae SHIROTSUKI ◽  
Xi ZHANG ◽  
Takanao ISHIKAWA ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Tridentate Ligands ◽  
Synthesis And Crystal Structure

Synthesis and Crystal Structure of a 6H Hexagonal Fluoro-Perovskite: RbMgF3

2020 ◽  
Author(s):  
Mohammad Usman ◽  
Gyanendra B. Ayer ◽  
Mark D. Smith ◽  
Hans-Conrad zur Loye
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure

Synthesis and crystal structure of BaSrCuO2+x·CO3

1992 ◽  
Vol 195 (3-4) ◽  
pp. 335-344 ◽  
Author(s):  
C. Chaillout ◽  
Q. Huang ◽  
R.J. Cava ◽  
J. Chenavas ◽  
A. Santoro ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Synthesis And Crystal Structure
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