Magnetic core–shell titanium dioxide nanoparticles as an efficient catalyst for domino Knoevenagel–Michael-cyclocondensation reaction of malononitrile, various aldehydes and dimedone

RSC Advances ◽  
2015 ◽  
Vol 5 (19) ◽  
pp. 14305-14310 ◽  
Author(s):  
Ardeshir Khazaei ◽  
Fatemeh Gholami ◽  
Vahid Khakyzadeh ◽  
Ahmad Reza Moosavi-Zare ◽  
Javad Afsar
Keyword(s):  
Titanium Dioxide ◽  
Titanium Dioxide Nanoparticles ◽  
Magnetic Core ◽  
Solvent Free ◽  
Core Shell ◽  
One Pot ◽  
Efficient Catalyst ◽  
Solvent Free Conditions ◽  
Three Component Reaction ◽  
Cyclocondensation Reaction

Fe3O4@SiO2@TiO2 efficiently catalysed the preparation of tetrahydrobenzo[b]pyrans by a one-pot three component reaction of aldehydes, dimedone and malononitrile at 100 °C under solvent-free conditions.

TiO2–SiO2 nanocomposite as a highly efficient catalyst for the solvent-free cyclocondensation reaction of isatins, cyclohexanones, and urea

2019 ◽  
Vol 74 (7-8) ◽  
pp. 559-564
Author(s):  
Simin Janitabar-Darzi ◽  
Shahrzad Abdolmohammadi
Keyword(s):  
Present Method ◽  
High Efficiency ◽  
Solvent Free ◽  
High Catalytic Activity ◽  
One Pot ◽  
Efficient Catalyst ◽  
Solvent Free Conditions ◽  
Cyclocondensation Reaction ◽  
The One ◽  
High Yields

AbstractA TiO2–SiO2 nanocomposite catalyzes the one-pot cyclocondensation reaction of 1H-indole-2,3-diones (isatins), 1,3-cyclohexanediones, and urea at T = 70°C under solvent-free conditions with high efficiency. The present method affords the corresponding spiro products in high yields and short reaction time. The unique features of the TiO2–SiO2 nanocomposite are high catalytic activity, ease of preparation, non-toxicity, low loading, and recyclability.

scholarly journals Trichloroisocyanuric acid, a New and Efficient Catalyst for the Synthesis of 2′- Aminobenzothiazolo-arylmethyl-2-naphthols

2012 ◽  
Vol 9 (4) ◽  
pp. 2424-2428 ◽  
Author(s):  
Limin Yang
Keyword(s):  
Aromatic Aldehydes ◽  
Catalytic Amount ◽  
Solvent Free ◽  
One Pot ◽  
Efficient Catalyst ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Three Component Reaction ◽  
Trichloroisocyanuric Acid

An efficient one-pot synthesis of 2′-aminobenzothiazolo-arylmethyl-2-naphthols is described. This involves the three-component reaction ofβ-naphthol, aromatic aldehydes and 2-aminobenzothiazole in the presence of a catalytic amount of trichloroisocyanuric acid under solvent-free conditions.

A novel inorganic–organic nanohybrid material H4SiW12O40/pyridino-MCM-41 as efficient catalyst for the preparation of 1-amidoalkyl-2-naphthols under solvent-free conditions

2015 ◽  
Vol 44 (20) ◽  
pp. 9596-9609 ◽  
Author(s):  
R. Tayebee ◽  
M. M. Amini ◽  
M. Akbari ◽  
A. Aliakbari
Keyword(s):  
Solvent Free ◽  
One Pot ◽  
Efficient Catalyst ◽  
Solvent Free Conditions ◽  
The One ◽  
Substituted 1 ◽  
Nanohybrid Material ◽  
Mcm 41

A new inorganic–organic nanohybrid material was prepared and performed as an efficient catalyst for the one-pot multi-component synthesis of different substituted 1-amidoalkyl-2-naphthols under solvent-free conditions.

scholarly journals One-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by SO3H@imineZCMNPs as a novel, efficient and reusable acidic nanocatalyst under solvent-free conditions

RSC Advances ◽  
2018 ◽  
Vol 8 (70) ◽  
pp. 40243-40251 ◽  
Author(s):  
Esmayeel Abbaspour-Gilandeh ◽  
Asieh Yahyazadeh ◽  
Mehraneh Aghaei-Hashjin
Keyword(s):  
Solvent Free ◽  
Magnetic Nanocatalyst ◽  
One Pot ◽  
Environment Friendly ◽  
Novel Environment ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
Three Component Reaction

The synthesis of 3,4-dihydropyrimidin-2(1H)-one derivatives was accomplished via a three-component reaction in the presence of SO3H@imineZCMNPs as a novel, environment friendly, and reusable heterogeneous magnetic nanocatalyst under solvent-free conditions at 90 °C.

CeCl3·7H2O as mild and efficient catalyst for the one-pot multicomponent synthesis of 8-aryl-7,8-dihydro[1,3]dioxolo[4,5-g]chromen-6-ones

2011 ◽  
Vol 76 (4) ◽  
pp. 235-241 ◽  
Author(s):  
Li-Qiang Wu ◽  
Wei-Lin Li ◽  
Fu-Lin Yan
Keyword(s):  
Aromatic Aldehydes ◽  
Environmentally Benign ◽  
Multicomponent Synthesis ◽  
One Pot ◽  
Efficient Catalyst ◽  
Solvent Free Conditions ◽  
Three Component Reaction ◽  
The One ◽  
High Yields ◽  
Work Up

A series of new 8-aryl-7,8-dihydro[1,3]dioxolo[4,5-g]chromen-6-ones were synthesized via a three-component reaction of 3,4-methylenedioxyphenol, aromatic aldehydes and Meldrum’s acid in the presence of CeCl3·7H2O under solvent-free conditions. The method provided several advantages such as easy work-up, high yields and environmentally benign procedure.

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