Ordered mesoporous crystalline aluminas from self-assembly of ABC triblock terpolymer–butanol–alumina sols

RSC Advances ◽  
2015 ◽  
Vol 5 (61) ◽  
pp. 49287-49294 ◽  
Author(s):  
Kwan Wee Tan ◽  
Hiroaki Sai ◽  
Spencer W. Robbins ◽  
Jörg G. Werner ◽  
Tobias N. Hoheisel ◽  
...  
Keyword(s):  
Self Assembly ◽  
One Pot ◽  
Structure Directing Agent ◽  
One Pot Synthesis ◽  
Ordered Mesoporous

One-pot synthesis of periodically mesostructured γ-alumina using an ABC triblock terpolymer as structure-directing agent and in situ derived rigid carbon scaffold.

One-pot synthesis of ordered mesoporous transition metal–zirconium oxophosphate composites with excellent textural and catalytic properties

2015 ◽  
Vol 39 (2) ◽  
pp. 1322-1329 ◽  
Author(s):  
Zhichao Miao ◽  
Huahua Zhao ◽  
Jian Yang ◽  
Jun Zhao ◽  
Huanling Song ◽  
...  
Keyword(s):  
Transition Metal ◽  
Self Assembly ◽  
Catalytic Properties ◽  
One Pot ◽  
One Pot Synthesis ◽  
Ordered Mesoporous ◽  
Evaporation Induced Self Assembly

A series of ordered M–X–ZrPO materials were successfully synthesized via a facile and general one-pot evaporation-induced self-assembly (EISA) strategy.

Direct one-pot synthesis of ordered mesoporous carbons from lignin with metal coordinated self-assembly

2021 ◽  
Author(s):  
Xiaoqi Wang ◽  
Xiaoning Liu ◽  
Richard Lee Smith ◽  
Yining Liang ◽  
Xinhua Qi
Keyword(s):  
Self Assembly ◽  
Agricultural Waste ◽  
Carbon Precursor ◽  
Mesoporous Carbons ◽  
One Pot ◽  
Ordered Mesoporous Carbons ◽  
Metal Ligands ◽  
One Pot Synthesis ◽  
Ordered Mesoporous ◽  
Evaporation Induced Self Assembly

This work reports one-pot synthesis of metal-linked OMCs, using lignin from agricultural waste sources as a sole carbon precursor, through coordinated interactions between lignin functional groups and metal ligands with classical solvent evaporation induced self-assembly.

Indium Bromide-catalyzed Unprecedented Hydrogenolysis: A Novel One-Pot Synthesis of Per-O-Acetylated β-carboxymethyl O and S-glycosides

2020 ◽  
Vol 24 (8) ◽  
pp. 900-908
Author(s):  
Ram Naresh Yadav ◽  
Amrendra K Singh ◽  
Bimal Banik
Keyword(s):  
Asymmetric Synthesis ◽  
Chiral Auxiliary ◽  
Bioactive Molecules ◽  
One Pot ◽  
Enantiomerically Pure ◽  
Stereoselective Glycosylation ◽  
One Pot Synthesis ◽  
Wide Range

Numerous O (oxa)- and S (thia)-glycosyl esters and their analogous glycosyl acids have been accomplished through stereoselective glycosylation of various peracetylated bromo sugar with benzyl glycolate using InBr3 as a glycosyl promotor followed by in situ hydrogenolysis of resulting glycosyl ester. A tandem glycosylating and hydrogenolytic activity of InBr3 has been successfully investigated in a one-pot procedure. The resulting synthetically valuable and virtually unexplored class of β-CMGL (glycosyl acids) could serve as an excellent potential chiral auxiliary in the asymmetric synthesis of a wide range of enantiomerically pure medicinally prevalent β-lactams and other bioactive molecules of diverse medicinal interest.

Hypervalent-Iodine Mediated One-Pot Synthesis of Isoxazolines and Isoxazoles bearing Difluoromethyl Phosphonate Moiety

2021 ◽  
Author(s):  
Romana Pajkert ◽  
Henryk Koroniak ◽  
Pawel Kafarski ◽  
Gerd Volker Roeschenthaler
Keyword(s):  
Nitrile Oxide ◽  
Dipolar Cycloaddition ◽  
Hypervalent Iodine ◽  
One Pot ◽  
One Pot Synthesis

A one-pot, regioselective 1,3-dipolar cycloaddition of in situ generated (diethoxyphosphoryl)difluoromethyl nitrile oxide toward selected alkenes and alkynes is reported. This protocol enables facile access to 3,5-disubstituted isoxazolines and isoxazoles bearing...

scholarly journals One-Pot Synthesis of Novel Multisubstituted 1-Alkoxyindoles

Molecules ◽  
2021 ◽  
Vol 26 (5) ◽  
pp. 1466
Author(s):  
Ye Eun Kim ◽  
Hyunsung Cho ◽  
Yoo Jin Lim ◽  
Chorong Kim ◽  
Sang Hyup Lee
Keyword(s):  
Alkyl Halide ◽  
The Novel ◽  
Reaction Conditions ◽  
One Pot ◽  
One Pot Synthesis ◽  
Consecutive Reactions ◽  
Intramolecular Condensation ◽  
Synthetic Sequence ◽  
Novel Target

Studies on a one-pot synthesis of novel multisubstituted 1-alkoxyindoles 1 and their mechanistic investigations are presented. The synthesis of 1 was successfully achieved through consecutive four step reactions from substrates 2. The substrates 2, prepared through a two-step synthetic sequence, underwent three consecutive reactions of nitro reduction, intramolecular condensation, and nucleophilic 1,5-addition to provide the intermediates, 1-hydroxyindoles 8, which then were alkylated in situ with alkyl halide to afford the novel target products 1. We optimized the reaction conditions for 1 focusing on the alkylation step, along with the consideration of formation of intermediates 8. The optimized condition was SnCl2·2H2O (3.3 eq) and alcohols (R1OH, 2.0 eq) for 1–2 h at 40 °C and then, base (10 eq) and alkyl halides (R2Y, 2.0 eq) for 1–4 h at 25–50 °C. Notably, all four step reactions were performed in one-pot to give 1 in good to modest yields. Furthermore, the mechanistic aspects were also discussed regarding the reaction pathways and the formation of side products. The significance lies in development of efficient one-pot reactions and in generation of new 1-alkoxyindoles.

One-Pot Synthesis and CO2 Adsorption Properties of Ordered Mesoporous SBA-15 Materials Functionalized with APTMS

2011 ◽  
Vol 115 (26) ◽  
pp. 12873-12882 ◽  
Author(s):  
Shiyou Hao ◽  
Hong Chang ◽  
Qiang Xiao ◽  
Yijun Zhong ◽  
Weidong Zhu
Keyword(s):  
Co2 Adsorption ◽  
Adsorption Properties ◽  
One Pot ◽  
One Pot Synthesis ◽  
Ordered Mesoporous

One-Pot Synthesis of ABC Type Triblock Copolymers via in situ Click [3 + 2] and Diels−Alder [4 + 2] Reactions

2007 ◽  
Vol 40 (2) ◽  
pp. 191-198 ◽  
Author(s):  
Hakan Durmaz ◽  
Aydan Dag ◽  
Ozcan Altintas ◽  
Tuba Erdogan ◽  
Gurkan Hizal ◽  
...  
Keyword(s):  
Triblock Copolymers ◽  
Diels Alder ◽  
One Pot ◽  
One Pot Synthesis

One-pot synthesis of a TiO2–CdS nano-heterostructure assembly with enhanced photocatalytic activity

RSC Advances ◽  
2015 ◽  
Vol 5 (44) ◽  
pp. 34942-34948 ◽  
Author(s):  
Sayantan Mazumdar ◽  
Aninda J. Bhattacharyya
Keyword(s):  
Titanium Dioxide ◽  
Photocatalytic Activity ◽  
Cadmium Sulfide ◽  
Self Assembly ◽  
Cost Effective ◽  
One Pot ◽  
One Pot Synthesis ◽  
Cost Effective Method

An unprecedented morphology of a titanium dioxide (TiO2) and cadmium sulfide (CdS) self-assembly obtained using a ‘truly’ one-pot and highly cost effective method with a multi-gram scale yield is reported here.

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