scholarly journals Applying multivariate analysis to x-ray diffraction computed tomography: the study of medieval applied brocades.

Author(s):  
Pierre Bordet ◽  
Florian Kergourlay ◽  
Ariane Pinto ◽  
NIls Blanc ◽  
Pauline Martinetto

X-ray diffraction tomography is a well-developed technique to study the structure of heterogeneous materials which makes it a tool of choice for the non-destructive investigation of cultural heritage microsamples. Characterizing...

2014 ◽  
Vol 27 ◽  
pp. 1460135
Author(s):  
CARMEN PAVEL ◽  
FLORIN CONSTANTIN ◽  
COSMIN IOAN SUCIU ◽  
ROXANA BUGOI

X-ray Computed Tomography (CT) is a powerful non-destructive technique that can yield interesting structural information not discernible through visual examination only. This paper presents the results of the CT scans of four objects belonging to the Romanian cultural heritage attributed to the Vinča, Cucuteni and Cruceni-Belegiš cultures. The study was performed with an X-ray tomographic device developed at the Department for Applied Nuclear Physics from Horia Hulubei National Institute for Nuclear Physics and Engineering in Măgurele, Romania. This apparatus was specially designed for archaeometric studies of low-Z artifacts: ceramic, wood, bone. The tomographic investigations revealed the internal configuration of the objects and provided information about the degree to which the previous manipulations affected the archaeological items. Based on the X-ray images resulting from the CT scans, hints about the techniques used in the manufacturing of the artifacts were obtained, as well as some indications useful for conservation/restoration purposes.


Talanta ◽  
2008 ◽  
Vol 76 (1) ◽  
pp. 183-188 ◽  
Author(s):  
A. Duran ◽  
L.K. Herrera ◽  
M.C. Jimenez de Haro ◽  
A. Justo ◽  
J.L. Perez-Rodriguez

2020 ◽  
Author(s):  
Eva Seknazi ◽  
Paul Zaslansky ◽  
Alex Katsman ◽  
Julie Villanova ◽  
Boaz Pokroy

AbstractThe dorsal arm plates (DAPs) of the Ophiocoma Wendtii brittle star are highly functional single crystalline biominerals whose optimized structure and nanostructure enable them to fullfill mechanical and optical functions in the organism. Here, a large DAP bulk piece is characterized by means of synchrotron X-ray Diffraction Tomography (XRDT). This non-destructive crystallographic characterization revealed an astounding feature: the presence of very high compressive strains which relax when the mineral is cracked or grinded into a powder. Thus, previous destructive characterization techniques did not allow their detection. We attribute the compressive strains to the previously identified high-Mg calcite particles, which are coherently included and thereby compress the low-Mg calcite matrix. The measured slice contained both the bulk DAP sample as well as DAP powder. The data generated by the bulk piece could be separated from those by the powder, and the latter was used to calibrate and interprete the former. This study reveals yet another awe-inspiring feature of a biogenic structure, highlights the importance of non-destructive crystallographic characterization for biominerals, and exemplifies the potential of XRDT use in studying a single crystalline material, as well as the advantage of complementary measurement of bulk and powder for data calibration and interpretation.


2003 ◽  
Vol 104 ◽  
pp. 27-30 ◽  
Author(s):  
T. Beetz ◽  
C. Jacobsen ◽  
C.-C. Kao ◽  
J. Kirz ◽  
O. Mentes ◽  
...  

Author(s):  
A. R. Lang

AbstractX-ray topography provides a non-destructive method of mapping point-by-point variations in orientation and reflecting power within crystals. The discovery, made by several workers independently, that in nearly perfect crystals it was possible to detect individual dislocations by X-ray diffraction contrast started an epoch of rapid exploitation of X-ray topography as a new, general method for assessing crystal perfection. Another discovery, that of X-ray Pendellösung, led to important theoretical developments in X-ray diffraction theory and to a new and precise method for measuring structure factors on an absolute scale. Other highlights picked out for mention are studies of Frank-Read dislocation sources, the discovery of long dislocation helices and lines of coaxial dislocation loops in aluminium, of internal magnetic domain structures in Fe-3 wt.% Si, and of stacking faults in silicon and natural diamonds.


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