One-Pot Synthesis of a Cyclic Pyrene Octamer from Two Bifunctionalized Pyrene Monomers

Synthesis ◽  
2020 ◽  
Vol 53 (02) ◽  
pp. 344-347
Author(s):  
Hiroko Yamada ◽  
Naoki Aratani ◽  
Peifeng Mei ◽  
Ryo Kurosaki ◽  
Akinobu Matsumoto
Keyword(s):  
Molecular Structure ◽  
Single Crystal ◽  
Diffraction Analysis ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
X Ray Diffraction ◽  
One Pot ◽  
X Ray ◽  
One Pot Synthesis ◽  
Cross Coupling Reaction

AbstractA 2,2′-tert-butyl-5,9-6′,8′-cyclooctameric pyrenylene ([8]CP) was synthesized by a one-pot Suzuki–Miyaura cross-coupling reaction from two kinds of bifunctionalized monomers, as a rare example of a cyclic octamer. The octameric molecular structure of [8]CP was revealed by single-crystal X-ray diffraction analysis.

ChemInform Abstract: One-Pot Synthesis of 1,3-Enynes with a CF3Group on the Terminal sp2Carbon by an Oxidative Sonogashira Cross-Coupling Reaction.

ChemInform ◽  
2016 ◽  
Vol 47 (2) ◽  
Author(s):  
Akari Ikeda ◽  
Masaaki Omote ◽  
Kana Kusumoto ◽  
Atsushi Tarui ◽  
Kazuyuki Sato ◽  
...  
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
One Pot ◽  
One Pot Synthesis ◽  
Cross Coupling Reaction

Two Zr−based heterometal−organic frameworks for efficient CO2 reduction under visible light

CrystEngComm ◽  
2021 ◽  
Author(s):  
Ying Wang ◽  
Yao-mei Fu ◽  
Si-qi You ◽  
xuexin Li ◽  
Xinlong Wang ◽  
...  
Keyword(s):  
Transition Metal ◽  
Visible Light ◽  
Single Crystal ◽  
Diffraction Analysis ◽  
Co2 Reduction ◽  
X Ray Diffraction ◽  
Transition Metal Cations ◽  
One Pot ◽  
X Ray ◽  
Secondary Building Units

Two new zirconium−based heterometal−organic frameworks, Zr3CP3−Mn (1) and Zr3CP3−Ni (2) constructed from [Cp3Zr3(μ3−O)(μ2−OH)3(IN)3] secondary building units and transition metal cations, were successfully synthesized through one−pot method. Single-crystal X-ray diffraction analysis...

Synthesis of Unsymmetrical Aza[7]helicenes by One-Pot Wittig–Heck and Photodehydrogenation Sequence

Synlett ◽  
2017 ◽  
Vol 28 (17) ◽  
pp. 2262-2266 ◽  
Author(s):  
Ashutosh Bedekar ◽  
Blessy Rajan
Keyword(s):  
Fluorescence Spectroscopy ◽  
Single Crystal ◽  
Diffraction Analysis ◽  
X Ray Diffraction ◽  
One Pot ◽  
X Ray ◽  
Stepwise Procedure

An efficient protocol for the synthesis of unsymmetrical aza[7]helicenes has been developed. The bis-styryl-type substrates for regiospecific photodehydrogenative oxidative double cyclization to give helicenes were prepared by a one-pot Wittig–Heck sequence as well as a stepwise procedure. The derivatives were characterized by single-crystal X-ray diffraction analysis and fluorescence spectroscopy.

One-Pot Synthesis of Conjugated (E)-Enynones via Two Types of Cross-Coupling Reaction

Synlett ◽  
2010 ◽  
Vol 2010 (16) ◽  
pp. 2461-2464 ◽  
Author(s):  
Masayuki Hoshi ◽  
Hirokazu Yamazaki ◽  
Mitsuhiro Okimoto
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
One Pot ◽  
One Pot Synthesis ◽  
Cross Coupling Reaction
Sign in / Sign up

Export Citation Format

Share Document