Detection of single macromolecules using a cryogenic particle detector coupled to a biopolymer mass spectrometer

1996 ◽  
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Damian Twerenbold ◽  
Jean‐Luc Vuilleumier ◽  
Daniel Gerber ◽  
Almut Tadsen ◽  
Ben van den Brandt ◽  
...  

1995 ◽  
Vol 5 (2) ◽  
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K.D. Irwin ◽  
S.W. Nam ◽  
B. Cabrera ◽  
B. Chugg ◽  
G.S. Park ◽  
...  


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C. W. Fink ◽  
...  


1994 ◽  
Vol 323 (1) ◽  
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P. Colling ◽  
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D. Dummer ◽  
M. Frank ◽  
...  




1987 ◽  
Vol 48 (C6) ◽  
pp. C6-577-C6-582 ◽  
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A. R. Waugh ◽  
D. R. Kingham ◽  
C. H. Richardson ◽  
M. Goff


2015 ◽  
Vol 21 (2(93)) ◽  
pp. 3-14 ◽  
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O.V. Dudnik ◽  
◽  
E.V. Kurbatov ◽  
V.O. Tarasov ◽  
L.A. Andryushenko ◽  
...  


2019 ◽  
Vol 85 (6) ◽  
pp. 11-24
Author(s):  
I. V. Nikolaeva ◽  
A. A. Kravchenko ◽  
S. V. Palessky ◽  
S. V. Nechepurenko ◽  
D. V. Semenova

Two methods — ICP-MS and ICP-AES are used for certification of the new reference material — needles of Siberian pine (NSP-1). Techniques of the analysis include decomposition of plant samples in two different ways: acid digestion in a microwave system MARS-5 and lithium metaborate fusion followed by ICP-MS and ICP-AES analysis of the solutions. Simultaneous determinations of all the elements were carried out in low, medium and high resolution using SF-mass-spectrometer ELEMENT and atomic-emission spectrometer IRIS Advantage with external calibrations and internal standards (In — ICP-MS, Sc —ICP-AES). Middle and high resolutions of ICP mass spectrometer were used for interference corrections. Data obtained by ICP-MS and ICP-AES with different decomposition techniques are in good agreement. The ICP-MS and ICP-AES techniques have been validated by the analysis of three plant reference materials: LB-1 (leaf of a birch), Tr-1 (grass mixture) and EK-1 (Canadian pondweed). These techniques were used for the determination of 38 elements in the new reference material NSP-1. Relative standard deviations for most of the determined elements were below 10%. Combination of ICP-MS and ICP-AES techniques for certification of the new reference material makes it possible to expand the set of elements to be determined and to reduce the total analysis time.



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