Facile synthesis and characterization of polyaniline (PANI) – Aluminium oxide (Al2O3) nanocomposites by using chemical oxidative polymerization

2021 ◽  
Author(s):  
Supriya Vyas ◽  
Ashutosh Shukla ◽  
Sugam Shivhare ◽  
Navneeta Upadhyay
Author(s):  
R. Rathore ◽  
Soni Sharma

Nanocomposite of copolymer of N-Methyl pyrrole (NMPy) and N, N-Dimethyl aniline (NDMA) doped with HCl was synthesized by chemical oxidative polymerization. APS was used as oxidant. The sample was characterized by FTIR, TGA, XRD and four probe method. FTIR confirms the formation of copolymer and its structure. XRD analysis shows the amorphous nature of polymer nanocomposite. The electrical conductivity of sample was measured by using four probe method. Size and surface morphology were demonstrated by SEM.


Author(s):  
Sang Nguyen Xuan

Polypyrrole (PPy) nanocomposites reinforced with zinc oxide (ZnO) nanorod and nano flower were fabricated by chemical oxidative polymerization method using an ammonium per-sulphate (APS, (NH4)2S2O8) as an oxidizing agent. The polymer nanocomposite were characterized by X-ray diffractometer (XRD), scanning electron microscopy (SEM), and Fourier transform infrared (FTIR). The results were compared with pure as-prepared PPy. The SEM images of the nanocomposites show homogeneous dispersion characteristics and different morphologies of ZnO structures such as rod and flower-like shapes.  In the FTIR spectra, composite samples showed characteristic peaks of PPy shifted to higher positions confirmed the interfacial interactions between ZnO and PPy matrix.


2017 ◽  
Vol 72 (4) ◽  
pp. 1007-1020 ◽  
Author(s):  
Wanar Kongkaew ◽  
Watchara Sangwan ◽  
Walaiporn Prissanaroon-Ouajai ◽  
Anuvat Sirivat

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