Investigation of structural phase transitions in perovskites using high energy synchrotron radiation

1995 ◽  
Vol 55 (1-4) ◽  
pp. 17-35 ◽  
Author(s):  
H. B. Neumann ◽  
H. F. Poulsen ◽  
U. Rütt ◽  
J. R. Schneider ◽  
M. v. Zimmermann
1990 ◽  
Vol 23 (6) ◽  
pp. 545-549 ◽  
Author(s):  
H. L. Bhat ◽  
S. M. Clark ◽  
A. El Korashy ◽  
K. J. Roberts

The design of a new microfurnace for use for Laue diffraction studies of solid-state transformations is described. The furnace operates in the temperature range 298–573 K with a thermal stability of about ± 0.1 K. The potential of the synchrotron-radiation Laue diffraction technique for studies of structural phase transitions is demonstrated. Experimental data on phase transitions in caesium periodate, potassium tetrachlorozincate and pentaerythritol are presented.


2013 ◽  
Vol 86 (9) ◽  
pp. 932-940 ◽  
Author(s):  
Krzysztof Dorywalski ◽  
Bohdan Andriyevsky ◽  
Michał Piasecki ◽  
Iwan Kityk ◽  
Christoph Cobet ◽  
...  

2018 ◽  
Vol 51 (3) ◽  
pp. 761-767 ◽  
Author(s):  
Tom Faske ◽  
Wolfgang Donner

This article reports the development and characterization of a laboratory-based high-resolution X-ray powder diffractometer equipped with a 5.5 T magnet and closed-cycle helium cryostat that is primarily designed for the investigation of magneto-structural phase transitions. Unique features of the diffractometer include the position-sensitive detector, allowing the collection of an entire diffraction pattern at once, and the high energy resolution with Mo Kα 1 radiation. The ability to utilize a lower energy resolution but higher photon flux by switching to an X-ray mirror monochromator makes it a versatile setup for a variety of compounds. In this contribution, details of the design and performance of the instrument are presented along with its specifications.


1991 ◽  
Vol 185-189 ◽  
pp. 895-896 ◽  
Author(s):  
S. Sugai ◽  
S. Hosoya ◽  
T. Kajitani ◽  
T. Fukuda ◽  
S. Onodera

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